Leaching of rare earths from fine-grained zirconosilicate ore

Leaching of rare earths Y, La and Ce by sulphuric acid from fine-grained zirconosilicate ore was investigated using Ta-guchi method of experimental design. An orthogonal array of L8, 27 which denotes 7 factors at 2 levels was chosen to consider the various factors relevant to the leaching process: b...

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Bibliographic Details
Published inJournal of rare earths Vol. 34; no. 9; pp. 908 - 916
Main Authors Lim, H., Ibana, D., Eksteen, J.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.09.2016
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Summary:Leaching of rare earths Y, La and Ce by sulphuric acid from fine-grained zirconosilicate ore was investigated using Ta-guchi method of experimental design. An orthogonal array of L8, 27 which denotes 7 factors at 2 levels was chosen to consider the various factors relevant to the leaching process: baking time, baking temperature, acid dosage, leaching time, leaching temperature, grind size and dilution. Statistical analysis showed that sulphation baking was a significant step for the leaching of rare earths from the whole-of-ore and optimized leaching of rare earths involved the following condition: baking for 3 h at 320 ℃ at 3.2 g acid/g ore acid dosage followed by water leaching at 20 ℃ for 1 h and dilution of 20 mL water/g ore using 300 um grind size. The effect of each leaching factor was also discussed.
Bibliography:Leaching of rare earths Y, La and Ce by sulphuric acid from fine-grained zirconosilicate ore was investigated using Ta-guchi method of experimental design. An orthogonal array of L8, 27 which denotes 7 factors at 2 levels was chosen to consider the various factors relevant to the leaching process: baking time, baking temperature, acid dosage, leaching time, leaching temperature, grind size and dilution. Statistical analysis showed that sulphation baking was a significant step for the leaching of rare earths from the whole-of-ore and optimized leaching of rare earths involved the following condition: baking for 3 h at 320 ℃ at 3.2 g acid/g ore acid dosage followed by water leaching at 20 ℃ for 1 h and dilution of 20 mL water/g ore using 300 um grind size. The effect of each leaching factor was also discussed.
11-2788/TF
rare earths; yttrium; lanthanum; cerium; zirconosilicate leaching; Taguchi
H. Lim D. lbana, J. Eksteen(1. Western Australia School of Mines, Curtin University, 7 Conlon Street, Waterford, 6152, Australia; 2. Mining and Metallurgy, Western Australia School of Mines, Locked Bag 17, Kalgoorlie, 6433, Australia)
ISSN:1002-0721
2509-4963
DOI:10.1016/S1002-0721(16)60114-X