Thermoplastic polyolefin based polymer – blend-layered double hydroxide nanocomposites

Layered double hydroxides (LDHs) are a new class of promising nanomaterials which improve the physicochemical properties of the polymer matrix. The present work deals with the preparation of nanocomposites of ethylene vinyl acetate (EVA-28)/low density polyethylene (LDPE) blend (1:1 by wt.) with var...

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Published inComposites science and technology Vol. 68; no. 15; pp. 3234 - 3239
Main Authors Kuila, T., Srivastava, S.K., Bhowmick, A.K., Saxena, A.K.
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier Ltd 01.12.2008
Elsevier
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Abstract Layered double hydroxides (LDHs) are a new class of promising nanomaterials which improve the physicochemical properties of the polymer matrix. The present work deals with the preparation of nanocomposites of ethylene vinyl acetate (EVA-28)/low density polyethylene (LDPE) blend (1:1 by wt.) with varying amounts of organomodified layered double hydroxide (DS-LDH) by solution blending. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) have been used to find out the dispersion of Mg–Al nanolayers in EVA/LDPE blend. This confirms complete exfoliation of Mg–Al nanolayers in EVA-28/LDPE/DS-LDH nanocomposites. The measurements of mechanical properties of these nanocomposites show maximum tensile strength for 3 wt.% of DS-LDH content. However, elongation at break for the nanocomposites remains lower for entire filler loading with respect to neat EVA/LDPE blend. Thermogravimetric analysis shows successive improvement in the thermal stability behavior of the nanocomposites with increasing the concentration of DS-LDH. The limiting oxygen index values are also improved with increasing DS-LDH concentration. Swelling property measurement shows that solvent resistance properties of the nanocomposites are better at low filler loading.
AbstractList Layered double hydroxides (LDHs) are a new class of promising nanomaterials which improve the physicochemical properties of the polymer matrix. The present work deals with the preparation of nanocomposites of ethylene vinyl acetate (EVA-28)/low density polyethylene (LDPE) blend (1:1 by wt.) with varying amounts of organomodified layered double hydroxide (DS-LDH) by solution blending. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) have been used to find out the dispersion of Mg-Al nanolayers in EVA/LDPE blend. This confirms complete exfoliation of Mg-Al nanolayers in EVA-28/LDPE/DS-LDH nanocomposites. The measurements of mechanical properties of these nanocomposites show maximum tensile strength for 3 wt.% of DS-LDH content. However, elongation at break for the nanocomposites remains lower for entire filler loading with respect to neat EVA/LDPE blend. Thermogravimetric analysis shows successive improvement in the thermal stability behavior of the nanocomposites with increasing the concentration of DS-LDH. The limiting oxygen index values are also improved with increasing DS-LDH concentration. Swelling property measurement shows that solvent resistance orooerties of the nanocomoosites are better at low filler loading.
Layered double hydroxides (LDHs) are a new class of promising nanomaterials which improve the physicochemical properties of the polymer matrix. The present work deals with the preparation of nanocomposites of ethylene vinyl acetate (EVA-28)/low density polyethylene (LDPE) blend (1:1 by wt.) with varying amounts of organomodified layered double hydroxide (DS-LDH) by solution blending. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) have been used to find out the dispersion of Mg–Al nanolayers in EVA/LDPE blend. This confirms complete exfoliation of Mg–Al nanolayers in EVA-28/LDPE/DS-LDH nanocomposites. The measurements of mechanical properties of these nanocomposites show maximum tensile strength for 3 wt.% of DS-LDH content. However, elongation at break for the nanocomposites remains lower for entire filler loading with respect to neat EVA/LDPE blend. Thermogravimetric analysis shows successive improvement in the thermal stability behavior of the nanocomposites with increasing the concentration of DS-LDH. The limiting oxygen index values are also improved with increasing DS-LDH concentration. Swelling property measurement shows that solvent resistance properties of the nanocomposites are better at low filler loading.
Author Kuila, T.
Saxena, A.K.
Srivastava, S.K.
Bhowmick, A.K.
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  givenname: A.K.
  surname: Saxena
  fullname: Saxena, A.K.
  organization: Defence Materials and Stores Research and Development Establishment, Kanpur 208013, India
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Issue 15
Keywords D. TGA
B. Mechanical properties
Nanocomposites
Blend
Layered double hydroxide
Polymer blends
Mechanical properties
Thermoplastic rubber
Dispersion reinforced material
Experimental study
Oxygen index
Composite material
Solvent resistance
Tensile strength
Thermal stability
Thermal properties
EVA
Aluminium Oxides
Low density ethylene polymer
Concentration effect
Olefin polymer
Nanocomposite
Chemical properties
Magnesium Oxides
Language English
License CC BY 4.0
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Snippet Layered double hydroxides (LDHs) are a new class of promising nanomaterials which improve the physicochemical properties of the polymer matrix. The present...
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SubjectTerms Applied sciences
B. Mechanical properties
Blend
Composites
D. TGA
Exact sciences and technology
Forms of application and semi-finished materials
Layered double hydroxide
Nanocomposites
Polymer industry, paints, wood
Technology of polymers
Title Thermoplastic polyolefin based polymer – blend-layered double hydroxide nanocomposites
URI https://dx.doi.org/10.1016/j.compscitech.2008.08.003
https://search.proquest.com/docview/32991924
Volume 68
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