Silver nanoparticles supported on polyethylene glycol/cellulose acetate ultrafiltration membranes: preparation and characterization of composite
In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylf...
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Published in | Cellulose (London) Vol. 24; no. 11; pp. 4997 - 5012 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Dordrecht
Springer Netherlands
01.11.2017
Springer Nature B.V |
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Abstract | In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or
N
-methyl-2-pyrrolidone, NMP). The Ag-NPs used in the
ex situ
method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like
Escherichia coli
and
Staphylococcus aureus
. By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the
ex situ
DMF NP composite membrane presented the highest amount of silver signals per unit area (µm
2
). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity. |
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AbstractList | In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or N-methyl-2-pyrrolidone, NMP). The Ag-NPs used in the ex situ method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like Escherichia coli and Staphylococcus aureus. By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the ex situ DMF NP composite membrane presented the highest amount of silver signals per unit area (µm2). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity. In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or N -methyl-2-pyrrolidone, NMP). The Ag-NPs used in the ex situ method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like Escherichia coli and Staphylococcus aureus . By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the ex situ DMF NP composite membrane presented the highest amount of silver signals per unit area (µm 2 ). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity. |
Author | Cadena-Nava, Rubén Darío Sotelo-Barrera, Erika Lis Núñez-Rivera, Alfredo Caloca, Jonathan Espinoza-Gomez, Heriberto Flores-López, Lucía Z. |
Author_xml | – sequence: 1 givenname: Jonathan surname: Caloca fullname: Caloca, Jonathan organization: Centro de Graduados e Investigación en Química, Instituto Tecnológico de Tijuana – sequence: 2 givenname: Lucía Z. orcidid: 0000-0001-5461-7573 surname: Flores-López fullname: Flores-López, Lucía Z. email: lzflores@hotmail.com organization: Centro de Graduados e Investigación en Química, Instituto Tecnológico de Tijuana – sequence: 3 givenname: Heriberto orcidid: 0000-0001-9398-7008 surname: Espinoza-Gomez fullname: Espinoza-Gomez, Heriberto email: hespinoza@uabc.edu.mx organization: Facultad de Ciencias Químicas e Ingeniería, Universidad Autónoma de Baja California – sequence: 4 givenname: Erika Lis surname: Sotelo-Barrera fullname: Sotelo-Barrera, Erika Lis organization: Centro de Nanociencias y Nanotecnología, Universidad Nacional Autónoma de México – sequence: 5 givenname: Alfredo surname: Núñez-Rivera fullname: Núñez-Rivera, Alfredo organization: Centro de Nanociencias y Nanotecnología, Universidad Nacional Autónoma de México – sequence: 6 givenname: Rubén Darío surname: Cadena-Nava fullname: Cadena-Nava, Rubén Darío organization: Centro de Nanociencias y Nanotecnología, Universidad Nacional Autónoma de México |
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CitedBy_id | crossref_primary_10_1016_j_apsusc_2019_06_031 crossref_primary_10_1016_j_ijbiomac_2024_131161 crossref_primary_10_1002_celc_202200173 crossref_primary_10_1016_j_jphotochem_2021_113481 crossref_primary_10_1016_j_apsusc_2020_147855 crossref_primary_10_1007_s10570_020_03250_2 crossref_primary_10_1016_j_watres_2022_118901 crossref_primary_10_1039_D1EN00941A crossref_primary_10_1016_j_microb_2024_100111 crossref_primary_10_1016_j_arabjc_2022_104053 crossref_primary_10_1002_slct_201803424 crossref_primary_10_1016_j_seppur_2018_08_075 |
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Keywords | in situ composite membranes ex situ composite membranes Ag-NPs/PEG/CA UF composite membranes Silver nanoparticles Silver nanoparticles supported |
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SubjectTerms | Bacteria Bioorganic Chemistry Cellulose acetate Ceramics Chemical synthesis Chemistry Chemistry and Materials Science Composites Dispersion E coli Fourier transforms Glass Infrared spectroscopy Membranes Molecular composites Morphology Nanoparticles Natural Materials Organic Chemistry Original Paper Particulate composites Permeability Physical Chemistry Polyethylene glycol Polyethylenes Polymer Sciences Scanning electron microscopy Silver Spectroscopic analysis Sustainable Development Thermogravimetric analysis Ultrafiltration |
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Title | Silver nanoparticles supported on polyethylene glycol/cellulose acetate ultrafiltration membranes: preparation and characterization of composite |
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