Silver nanoparticles supported on polyethylene glycol/cellulose acetate ultrafiltration membranes: preparation and characterization of composite

In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylf...

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Published inCellulose (London) Vol. 24; no. 11; pp. 4997 - 5012
Main Authors Caloca, Jonathan, Flores-López, Lucía Z., Espinoza-Gomez, Heriberto, Sotelo-Barrera, Erika Lis, Núñez-Rivera, Alfredo, Cadena-Nava, Rubén Darío
Format Journal Article
LanguageEnglish
Published Dordrecht Springer Netherlands 01.11.2017
Springer Nature B.V
Subjects
Bacteria
Bioorganic Chemistry
Cellulose acetate
Ceramics
Chemical synthesis
Chemistry
Chemistry and Materials Science
Composites
Dispersion
E coli
Fourier transforms
Glass
Infrared spectroscopy
Membranes
Molecular composites
Morphology
Nanoparticles
Natural Materials
Organic Chemistry
Original Paper
Particulate composites
Permeability
Physical Chemistry
Polyethylene glycol
Polyethylenes
Polymer Sciences
Scanning electron microscopy
Silver
Spectroscopic analysis
Sustainable Development
Thermogravimetric analysis
Ultrafiltration
in situ composite membranes
ex situ composite membranes
Ag-NPs/PEG/CA UF composite membranes
Silver nanoparticles
Silver nanoparticles supported
Online AccessGet full text

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Abstract In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or N -methyl-2-pyrrolidone, NMP). The Ag-NPs used in the ex situ method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like Escherichia coli and Staphylococcus aureus . By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the ex situ DMF NP composite membrane presented the highest amount of silver signals per unit area (µm 2 ). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity.
AbstractList In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or N-methyl-2-pyrrolidone, NMP). The Ag-NPs used in the ex situ method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like Escherichia coli and Staphylococcus aureus. By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the ex situ DMF NP composite membrane presented the highest amount of silver signals per unit area (µm2). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity.
In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and characterized. The Ag-NPs were embedded in the polymer matrix by two methods: in situ and ex situ; varying the type of solvent used (dimethylformamide, DMF; or N -methyl-2-pyrrolidone, NMP). The Ag-NPs used in the ex situ method were synthesized by a green chemistry reduction method. The composite membranes were characterized by Fourier transform infrared spectroscopy with attenuated total reflection (FTIR-ATR), scanning electron microscopy with energy dispersive spectroscopy (SEM-EDS), and thermogravimetric analysis-derivative thermogravimetric analysis (TGA-DTG); the molecular weight cut-off and permeability were also determined. Moreover, the antibacterial efficiency of the composite membranes was measured against bacteria like Escherichia coli and Staphylococcus aureus . By FTIR-ATR analysis it was possible to observe that the Ag-NPs embedded in membranes changed the membrane morphology. The SEM-EDS analysis showed that the in situ composite membranes have good dispersity of Ag-NPs, DMF FB being the most densely populated obtained. By another hand, the ex situ DMF NP composite membrane presented the highest amount of silver signals per unit area (µm 2 ). The permeability of the membrane was affected by the presence of the Ag-NPs; the DMF NP composite membrane had the highest permeate flow, while DMF FB had the highest antibacterial activity.
Author Cadena-Nava, Rubén Darío
Sotelo-Barrera, Erika Lis
Núñez-Rivera, Alfredo
Caloca, Jonathan
Espinoza-Gomez, Heriberto
Flores-López, Lucía Z.
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Issue 11
Keywords in situ composite membranes
ex situ composite membranes
Ag-NPs/PEG/CA UF composite membranes
Silver nanoparticles
Silver nanoparticles supported
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Snippet In this research work, silver nanoparticles/polyethylene glycol/cellulose acetate ultrafiltration (Ag-NPs/PEG/CA UF) composite membranes were synthesized and...
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SubjectTerms Bacteria
Bioorganic Chemistry
Cellulose acetate
Ceramics
Chemical synthesis
Chemistry
Chemistry and Materials Science
Composites
Dispersion
E coli
Fourier transforms
Glass
Infrared spectroscopy
Membranes
Molecular composites
Morphology
Nanoparticles
Natural Materials
Organic Chemistry
Original Paper
Particulate composites
Permeability
Physical Chemistry
Polyethylene glycol
Polyethylenes
Polymer Sciences
Scanning electron microscopy
Silver
Spectroscopic analysis
Sustainable Development
Thermogravimetric analysis
Ultrafiltration
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Title Silver nanoparticles supported on polyethylene glycol/cellulose acetate ultrafiltration membranes: preparation and characterization of composite
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