A Novel Metal-free Reductive Esterification of N-Tosylhydrazones with Carboxylic Acids
A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed. Various functional groups were found to be tolerable under the re- action conditions to afford low to good yields.
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| Published in | Chinese journal of chemistry Vol. 30; no. 8; pp. 1862 - 1866 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.08.2012
WILEY‐VCH Verlag Wiley Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1001-604X 1614-7065 |
| DOI | 10.1002/cjoc.201200387 |
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| Abstract | A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed. Various functional groups were found to be tolerable under the re- action conditions to afford low to good yields. |
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| AbstractList | A novel method for the synthesis of esters via reductive coupling of
N
‐tosylhydrazones with carboxylic acids under metal‐free conditions has been developed. Various functional groups were found to be tolerable under the reaction conditions to afford low to good yields. A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed. Various functional groups were found to be tolerable under the re- action conditions to afford low to good yields. A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed. Various functional groups were found to be tolerable under the reaction conditions to afford low to good yields. A novel method for the synthesis of esters via reductive coupling of N‐tosylhydrazones with carboxylic acids under metal‐free conditions has been developed. Various functional groups were found to be tolerable under the reaction conditions to afford low to good yields. A novel method for the synthesis of esters via reductive coupling of N‐tosylhydrazones with carboxylic acids under metal‐free conditions has been developed. Various functional groups were found to be tolerable under the reaction conditions to afford up to 89% yield. |
| Author | Zhang, Xiao Zhou, Ankun Li, Dazhi Xia, Wujiong Chen, Qingqing Wu, Lei |
| AuthorAffiliation | State Key Lab of Urban Water Resource and Environment, the Academy of Fundamental and Interdisciplinary Sciences, Harbin Institute of Technology, Harbin, Heilongjiang 150080, China |
| Author_xml | – sequence: 1 fullname: 周安坤 吴磊 李大志 陈庆庆 张晓 夏吾炯 |
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| Cites_doi | 10.1016/j.tetlet.2010.12.093 10.1002/anie.201106825 10.1021/ol103009n 10.1039/C1CS15127D 10.1016/j.tetlet.2009.09.046 10.1038/nchem.328 10.1002/anie.200906349 10.1002/anie.201001704 10.1039/C0OB00639D 10.1002/anie.201005741 10.1002/anie.200701815 10.1002/anie.201108139 10.1039/c0ob00639d 10.1038/NCHEM.328 10.1002/anie.201006595 10.1039/c1cs15127d |
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| Copyright | Copyright © 2012 SIOC, CAS, Shanghai & WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim Copyright © 2012 SIOC, CAS, Shanghai & WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim |
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| Keywords | esterification metal-free N-tosylhydrazones carboxylic acids |
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| Notes | 31-1547/O6 Zhou Ankun,Wu Lei, Li Dazhi, Chen Qingqing,Zhang Xiao,Xia Wujiong（ State Key Lab of Urban Water Resource and Environment, the Academy of Fundamental and Interdisciplinary Sciences, Harbin Institute of Technology, Harbin, Heilongjiang 150080, China） metal-free, N-tosylhydrazones, esterification, carboxylic acids A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed. Various functional groups were found to be tolerable under the re- action conditions to afford low to good yields. the China Postdoctoral Science Foundation - No. 2011M500096 Harbin Institute of Technology ArticleID:CJOC201200387 ark:/67375/WNG-LMKNK04W-8 istex:E96386DE4DCD2EECF1504CA0196454F104EF7792 Natural Scientific Research Innovation Foundation in Harbin Institute of Technology - No. HIT.NSRIF 2010054 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 |
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| Snippet | A novel method for the synthesis of esters via reductive coupling of N-tosylhydrazones with carboxylic acids under metal-free conditions has been developed.... A novel method for the synthesis of esters via reductive coupling of N‐tosylhydrazones with carboxylic acids under metal‐free conditions has been developed.... A novel method for the synthesis of esters via reductive coupling of N ‐tosylhydrazones with carboxylic acids under metal‐free conditions has been developed.... |
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| SubjectTerms | Acids Carboxylic acids Chemistry Chemistry, Multidisciplinary esterification Esters metal-free N-tosylhydrazones Physical Sciences Science & Technology 官能团 羧酸 还原偶联 酯化反应 金属条 |
| Title | A Novel Metal-free Reductive Esterification of N-Tosylhydrazones with Carboxylic Acids |
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