Preparation of zeolite NaA for CO2 capture from nickel laterite residue

Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range of experimental techniques, such as X-ray diffraction, scanning electronic microsc...

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Published inInternational journal of minerals, metallurgy and materials Vol. 21; no. 8; pp. 820 - 825
Main Authors Du, Tao, Liu, Li-ying, Xiao, Penny, Che, Shuai, Wang, He-ming
Format Journal Article
LanguageEnglish
Published Beijing University of Science and Technology Beijing 01.08.2014
Springer Nature B.V
School of Material and Metal urgy, Northeastern University, Shenyang 110819, China%Department of Chemical and Biomolecular Engineering, The University of Melbourne, VIC 3010, Australia
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Summary:Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range of experimental techniques, such as X-ray diffraction, scanning electronic microscopy, and infrared spectroscopy. It was revealed that the structures of the produced zeolites were dependent on the molar ratios of the reactants and hydrothermal reaction conditions, so the synthesis conditions were optimized to obtain pure zeolite NaA. Adsorption of nitrogen and carbon dioxide on the prepared zeolite NaA was also measured and analyzed. The results showed that zeolite NaA could be prepared with reasonable purity, it had physicochemical properties comparable with zeolite NaA made from other methods, and it had excellent gas adsorption properties, thus demonstrating that zeolite NaA could be prepared from nickel laterite residue.
Bibliography:zeolites; nickel laterite; residue; synthesis; structural properties; carbon dioxide; adsorption
Zeolite NaA was successfully prepared from nickel laterite residue for the first time via a fusion-hydrothermal procedure. The structure and morphology of the as-synthesized zeolite NaA were characterized with a range of experimental techniques, such as X-ray diffraction, scanning electronic microscopy, and infrared spectroscopy. It was revealed that the structures of the produced zeolites were dependent on the molar ratios of the reactants and hydrothermal reaction conditions, so the synthesis conditions were optimized to obtain pure zeolite NaA. Adsorption of nitrogen and carbon dioxide on the prepared zeolite NaA was also measured and analyzed. The results showed that zeolite NaA could be prepared with reasonable purity, it had physicochemical properties comparable with zeolite NaA made from other methods, and it had excellent gas adsorption properties, thus demonstrating that zeolite NaA could be prepared from nickel laterite residue.
11-5787/T
ISSN:1674-4799
1869-103X
DOI:10.1007/s12613-014-0976-8