Aging of electrochemical double layer capacitors with acetonitrile-based electrolyte at elevated voltages
Laboratory-scale electrochemical capacitor cells with bound activated carbon electrodes and acetonitrile-based electrolyte were aged at various elevated constant cell voltages between 2.75 V and 4.0 V. During the constant voltage tests, the cell capacitance as well as the capacitance and resistance...
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| Published in | Electrochimica acta Vol. 55; no. 15; pp. 4412 - 4420 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.06.2010
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Laboratory-scale electrochemical capacitor cells with bound activated carbon electrodes and acetonitrile-based electrolyte were aged at various elevated constant cell voltages between 2.75
V and 4.0
V. During the constant voltage tests, the cell capacitance as well as the capacitance and resistance of each electrode was determined. Following each aging experiment, the cells were analyzed by means of electrochemical impedance spectroscopy, and the individual electrodes were characterized by gas adsorption and X-ray photoelectron spectroscopy. At cell voltages above 3.0
V, the positive electrode ages much faster than the negative. Both the capacitance loss and resistance increase of the cell could be totally attributed to the positive electrode. At cell voltages above 3.5
V also the negative electrode aged significantly. X-ray photoelectron spectroscopy indicated the presence of degradation products on the electrode surface with a much thicker layer on the positive electrode. Simultaneously, a significant decrease in electrode porosity could be detected by gas adsorption. |
|---|---|
| AbstractList | Laboratory-scale electrochemical capacitor cells with bound activated carbon electrodes and acetonitrile-based electrolyte were aged at various elevated constant cell voltages between 2.75 V and 4.0 V. During the constant voltage tests, the cell capacitance as well as the capacitance and resistance of each electrode was determined. Following each aging experiment, the cells were analyzed by means of electrochemical impedance spectroscopy, and the individual electrodes were characterized by gas adsorption and X-ray photoelectron spectroscopy. At cell voltages above 3.0 V, the positive electrode ages much faster than the negative. Both the capacitance loss and resistance increase of the cell could be totally attributed to the positive electrode. At cell voltages above 3.5 V also the negative electrode aged significantly. X-ray photoelectron spectroscopy indicated the presence of degradation products on the electrode surface with a much thicker layer on the positive electrode. Simultaneously, a significant decrease in electrode porosity could be detected by gas adsorption. Laboratory-scale electrochemical capacitor cells with bound activated carbon electrodes and acetonitrile-based electrolyte were aged at various elevated constant cell voltages between 2.75 V and 4.0 V. During the constant voltage tests, the cell capacitance as well as the capacitance and resistance of each electrode was determined. Following each aging experiment, the cells were analyzed by means of electrochemical impedance spectroscopy, and the individual electrodes were characterized by gas adsorption and X-ray photoelectron spectroscopy. At cell voltages above 3.0 V, the positive electrode ages much faster than the negative. Both the capacitance loss and resistance increase of the cell could be totally attributed to the positive electrode. At cell voltages above 3.5 V also the negative electrode aged significantly. X-ray photoelectron spectroscopy indicated the presence of degradation products on the electrode surface with a much thicker layer on the positive electrode. Simultaneously, a significant decrease in electrode porosity could be detected by gas adsorption. |
| Author | Foelske-Schmitz, A. Kötz, R. Cericola, D. Wokaun, A. Ruch, P.W. |
| Author_xml | – sequence: 1 givenname: P.W. surname: Ruch fullname: Ruch, P.W. – sequence: 2 givenname: D. surname: Cericola fullname: Cericola, D. – sequence: 3 givenname: A. surname: Foelske-Schmitz fullname: Foelske-Schmitz, A. – sequence: 4 givenname: R. surname: Kötz fullname: Kötz, R. email: ruediger.koetz@psi.ch – sequence: 5 givenname: A. surname: Wokaun fullname: Wokaun, A. |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22727918$$DView record in Pascal Francis |
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| Issue | 15 |
| Keywords | Degradation Supercapacitors Double layer capacitance Non-aqueous electrolyte Activated carbon Specific surface area X ray Electrolytic capacitor Electrodes Electrolyte Acetonitrile Voltage Surface properties Supercapacitor Artificial ageing Capacitance Photoelectron spectrometry Non aqueous solvent |
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| Snippet | Laboratory-scale electrochemical capacitor cells with bound activated carbon electrodes and acetonitrile-based electrolyte were aged at various elevated... |
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| SubjectTerms | Activated carbon Applied sciences Capacitance Capacitors Capacitors. Resistors. Filters Degradation Double layer capacitance Electric potential Electrical engineering. Electrical power engineering Electrodes Electrolytic cells Elevated Exact sciences and technology Non-aqueous electrolyte Supercapacitors Surface chemistry Various equipment and components Voltage |
| Title | Aging of electrochemical double layer capacitors with acetonitrile-based electrolyte at elevated voltages |
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