2-[Difluoro(phenylselenyl)methyl]benzo-1,3-thiazole

This short note elaborates a concise protocol for the synthesis of 2-[difluoro(phenylselenyl)methyl]benzo-1,3-thiazole in two steps from the commercially available reagent 2-aminobenzenethiol. The structures of the synthesized compounds are confirmed by 1H-NMR, 13C-NMR and 19F-NMR spectroscopy, infr...

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Bibliographic Details
Published inMolBank Vol. 2022; no. 4; p. M1450
Main Authors Xu, Rongfu, Cai, Ying, Liao, Fumin, Liu, Jinbiao
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 01.09.2022
Subjects
2-aminobenzenethiol
Analysis
bromodifluoroacetic acid
Cancer
Chemical synthesis
Chemistry
Chromatography
Conflicts of interest
diphenyl diselenide
Identification and classification
Infrared spectra
Infrared spectroscopy
Mass spectrometry
Methods
Natural products
NMR spectroscopy
Nuclear magnetic resonance spectroscopy
Pharmaceutical sciences
Reagents
Scientific imaging
Structure
Thiazoles
China
United States > US
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Summary:This short note elaborates a concise protocol for the synthesis of 2-[difluoro(phenylselenyl)methyl]benzo-1,3-thiazole in two steps from the commercially available reagent 2-aminobenzenethiol. The structures of the synthesized compounds are confirmed by 1H-NMR, 13C-NMR and 19F-NMR spectroscopy, infrared (IR) spectra, and high-resolution mass spectrometry.
ISSN:1422-8599
1422-8599
DOI:10.3390/M1450