Empirical model to predict mass gain of cobalt electroless deposition on ceramic particles using response surface methodology

This investigation was undertaken to predict the mass gain （MG） of cobalt electroless deposition （ED） on ceramic SiC particles.Response surface methodology （RSM） based on a full factorial design with three ED parameters and 30 runs was used to conduct the experiments and to establish a mathematical...

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Published inRare metals Vol. 36; no. 3; pp. 209 - 219
Main Authors Heidarzadeh, Akbar, Mousavian, Reza Taherzadeh, Khosroshahi, Rasoul Azari, Afkham, Yalda A., Pouraliakbar, Hesam
Format Journal Article
LanguageEnglish
Published Beijing Nonferrous Metals Society of China 01.03.2017
Springer Nature B.V
Subjects
Biomaterials
Ceramics
Chemistry and Materials Science
Cobalt
Copper
Design analysis
Design of experiments
Electroless deposition
Electroless plating
Energy
Factorial design
Gain
Heat treatment
Investigations
Materials Engineering
Materials Science
Mathematical models
Metallic Materials
Metals
Morphology
Nanoscale Science and Technology
Nickel
Parameters
Particle physics
Physical Chemistry
Response surface methodology
Silicon carbide
Temperature
Variance analysis
低pH值
化学镀钴
响应面法
扫描电子显微镜
经验模型
质量
陶瓷颗粒
预测模型
SiC particles
Mathematical model
Response surface method
Cobalt
Electroless deposition
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ISSN1001-0521
1867-7185
DOI10.1007/s12598-015-0564-8

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Summary:This investigation was undertaken to predict the mass gain （MG） of cobalt electroless deposition （ED） on ceramic SiC particles.Response surface methodology （RSM） based on a full factorial design with three ED parameters and 30 runs was used to conduct the experiments and to establish a mathematical model by means of Design-Expert software.Three ED parameters considered were pH,bath temperature and ceramic particle morphology.Analysis of variance was applied to validate the predicted model.The results of confirmation analysis by scanning electron microscopy （SEM） show that the developed models are reasonably accurate.The pH is the most effective parameter for the MG.Also,the highest mass gain is obtained for the lowest pH,highest bath temperatures and heat-treated SiC particles.In addition,the developed model shows that the optimal parameters to get a maximum value of mass gain are pH,bath temperature and ceramic particle state of 8,70 ℃ and heat treatment,respectively.
Bibliography:Electroless deposition; Cobalt; SiC particles;Mathematical model; Response surface method
This investigation was undertaken to predict the mass gain （MG） of cobalt electroless deposition （ED） on ceramic SiC particles.Response surface methodology （RSM） based on a full factorial design with three ED parameters and 30 runs was used to conduct the experiments and to establish a mathematical model by means of Design-Expert software.Three ED parameters considered were pH,bath temperature and ceramic particle morphology.Analysis of variance was applied to validate the predicted model.The results of confirmation analysis by scanning electron microscopy （SEM） show that the developed models are reasonably accurate.The pH is the most effective parameter for the MG.Also,the highest mass gain is obtained for the lowest pH,highest bath temperatures and heat-treated SiC particles.In addition,the developed model shows that the optimal parameters to get a maximum value of mass gain are pH,bath temperature and ceramic particle state of 8,70 ℃ and heat treatment,respectively.
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ISSN:1001-0521
1867-7185
DOI:10.1007/s12598-015-0564-8