Increased structural stability in twin-roll cast AZ31 magnesium alloy processed by equal channel angular pressing

• Published in: Materials characterization Vol. 153; pp. 199 - 207
• Main Authors: Minárik, P., Zimina, M., Čížek, J., Stráska, J., Krajňák, T., Cieslar, M., Vlasák, T., Bohlen, J., Kurz, G., Letzig, D.
• Format: Journal Article
• Language: English
• Published: Elsevier Inc 01.07.2019
• Subjects: ECAP; Magnesium; Microstructure; Thermal stability; Twin-roll casting; Twin-roll casting; Magnesium; Microstructure; ECAP; Thermal stability
• ISSN: 1044-5803; 1873-4189
• DOI: 10.1016/j.matchar.2019.05.006

The present paper reports an effect of ECAP on the microstructure of the AZ31 magnesium alloy prepared in two conditions: conventionally cast and twin-roll cast. Subsequently, the thermal stability of fine-grained conditions was investigated with a special regard to microhardness, grain structure and dislocation density changes. Similar processing conditions of ECAP resulted in achieving similar average grain size for both initial conditions regardless differences in the initial microstructure. The only difference in the microstructure of a fine-grained condition was a distribution of β-Al12Mg17 secondary phase particles. Isochronal annealing in the temperature range 160–500 °C showed differences in the response of individual fine-grained samples to the temperature increase. It was proven that these differences primarily originated from the different distribution of secondary phase particles, which significantly affected static recovery and grain growth. Consequently, the thermal stability of fine-grained structure was much better in twin-roll cast samples in the temperature range 220–340 °C. Exceeding 340 °C, accelerated dissolution of β-Al12Mg17 phase resulted in a similar evolution of all studied parameters showing that distribution of secondary phase particles is a crucial parameter of thermal stability of fine-grained AZ31 magnesium alloy. •After ECAP, comparable grain size, hardness and dislocation density•Different distribution of beta-phase after ECAP due to initial microstructure•Differences in recovery and grain growth during isochronal annealing up to 500 °C•TRC-8P, higher thermal stability of fine-grained microstructure between 220 and 340 °C