Ulva fasciata-mediated preparation of zinc oxide nanocrystalline for one-pot multicomponent synthesis of 6-amino-3-methyl-4-phenyl-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitrile

ZnO has been successfully prepared by a simple co-precipitation method using sodium hydroxide, zinc acetate as precursor and Ulva fasciata polysaccharides as capping agent. Characterization using FTIR, XRD and SEM-EDS indicated the successful formation of ZnO nanocrystalline with crystallite size of...

Full description

Saved in:
Bibliographic Details
Published inIOP conference series. Materials Science and Engineering Vol. 188; no. 1; pp. 12053 - 12059
Main Authors Cahyana, A H, Nurhayati, Utomo, B S B, Ardiansah, B
Format Journal Article
LanguageEnglish
Published Bristol IOP Publishing 01.04.2017
Subjects
Aqueous solutions
Crystallites
Nanocrystals
Polysaccharides
Pyrazole
Reaction time
Room temperature
Sodium hydroxide
Zinc acetate
Zinc oxide
Zinc oxides
Online AccessGet full text

Cover

More Information
Summary:ZnO has been successfully prepared by a simple co-precipitation method using sodium hydroxide, zinc acetate as precursor and Ulva fasciata polysaccharides as capping agent. Characterization using FTIR, XRD and SEM-EDS indicated the successful formation of ZnO nanocrystalline with crystallite size of 27.01 nm. In order to promote ZnO as a green catalyst, its application for one-pot multicomponent pyranopyrazole synthesis has been performed. Several reaction conditions have been investigated, and the highest yield (98%) was observed in the use of 10% mole of ZnO at room temperature for 90 min reaction time in aqueous medium to produce 6-amino-3-methyl-4-phenyl-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitrile.
ISSN:1757-8981
1757-899X
DOI:10.1088/1757-899X/188/1/012053