Effect of the severe plastic deformation by ECAP on microstructure and phase transformations in Ti-15Mo alloy

• Published in: Materials today communications Vol. 22; p. 100811
• Main Authors: Bartha, K., Veverková, A., Stráský, J., Veselý, J., Minárik, P., Corrêa, C.A., Polyakova, V., Semenova, I., Janeček, M.
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.03.2020
• Subjects: Equal channel angular pressing; Metastable β titanium alloy; Microstructure; Phase composition; Transmission Kikuchi diffraction; α phase precipitation; Transmission Kikuchi diffraction; α phase precipitation; Phase composition; Equal channel angular pressing; Microstructure; Metastable β titanium alloy
• ISSN: 2352-4928; 2352-4928
• DOI: 10.1016/j.mtcomm.2019.100811

•The Ti-15Mo alloy was deformed by ECAP processing at the temperature of 250 °C.•The shear bands created during ECAP contain a high density of lattice defects.•Shear bands/defects accelerate the α precipitation upon ageing.•The α particles are fine-grained and equiaxed in ECAP deformed material. Ti-15Mo alloy in a metastable β solution treated condition was processed by equal channel angular pressing (ECAP) at an elevated temperature of 250 °C. The resulting microstructure is highly deformed, contains twins and shear bands, but is not ultra-fine grained. Both the initial solution treated material and the material after ECAP were subjected to ageing at 400 °C and 500 °C in order to study the effect of deformation on phase transformations, namely the α phase precipitation. The phase composition was studied by X-ray diffraction measurement; the microstructure was investigated using conventional EBSD and an advanced method of transmission Kikuchi diffraction (TKD). It was shown that the α phase precipitation is accelerated in areas with higher density of lattice defects, which provide a dense net of preferred sites for nucleation and also fast diffusion paths necessary for accelerated growth. Upon further annealing, discontinuous lamellar coarsening occurs, which had not been previously reported in metastable β-Ti alloys. The microhardness is governed mainly by the formation of ω phase particles. The fraction of ω phase increases during annealing at 400 °C and the specimen aged at 400 °C/16 h shows the highest value of microhardness of 520 HV for both ECAP and undeformed material. Upon annealing at 500 °C, the microhardness is significantly lower.