In situ neutron diffraction study on temperature dependent deformation mechanisms of ultrafine grained austenitic Fe–14Cr–16Ni alloy

• Published in: International journal of plasticity Vol. 53; pp. 125 - 134
• Main Authors: Sun, C., Brown, D.W., Clausen, B., Foley, D.C., Yu, K.Y., Chen, Y., Maloy, S.A., Hartwig, K.T., Wang, H., Zhang, X.
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.02.2014
• Subjects: Austenitic stainless steels; Deformation mechanisms; Deviation; Dislocations; Grain boundaries; In situ neutron diffraction; Lattice strain; Neutron diffraction; Nonlinear dynamics; Reduction; Temperature effect; Ultrafine grained Fe–Cr–Ni; Temperature effect; Ultrafine grained Fe–Cr–Ni; Deformation mechanisms; In situ neutron diffraction
• ISSN: 0749-6419; 1879-2154
• DOI: 10.1016/j.ijplas.2013.07.007

•UFG austenitic Fe–Cr–Ni alloy shows diminished ductility as temperature increases up to 200°C.•Tensile deviation on [200] occurs before yielding by a larger margin at 200°C as revealed by in situ neutron diffraction studies.•A greater anisotropic distortion of crystal structure is observed with increasing temperature.•Dynamic recovery process expedites at elevated temperature. Using in situ neutron diffraction technique we investigated the temperature dependent deformation mechanisms in ultrafine grained (UFG) austenitic Fe–14Cr–16Ni alloy prepared by equal channel angular pressing. Tensile test studies show diminished ductility when testing temperature increased from 20 to 200°C. At 200°C, non-linear lattice strain deviation on [200] orientation proceeded plastic yielding by a large margin, accompanied by a greater distortion of crystal structure. In addition, the capability to accumulate dislocations was substantially reduced at 200°C as evidenced by lower dislocation density than that at 20°C. Dynamic recovery expedited at elevated temperature because of enlarged critical separation distance for annihilation of dislocation dipoles via climb. Calculations show that both high angle grain boundaries and thermal kinetic energy assisted the reduction of vacancy formation energy.