Microencapsulation of vanilla (Vanilla planifolia Andrews) and powder characterization

• Published in: Powder technology Vol. 323; pp. 416 - 423
• Main Authors: Calva-Estrada, S.J., Mendoza, M.R., García, O., Jiménez-Fernández, V.M., Jiménez, M.
• Format: Journal Article
• Language: English
• Published: Lausanne Elsevier B.V 01.01.2018; Elsevier BV
• Subjects: Antioxidant activity; Antioxidants; Dehydration; Drying; Flowers & plants; Food additives; Functional foods & nutraceuticals; Microcapsules; Microencapsulation; Microparticles; Microstructure; Physicochemical properties; Polyphenols; Powder; Retention; Shelf life; Spray-drying; Storage; Vanillin; Volatile compounds; Volatility; Whey; Whey protein; Whey protein concentrate; Whey protein concentrate; Volatile compounds; Vanillin; Spray-drying; Antioxidant activity
• ISSN: 0032-5910; 1873-328X
• DOI: 10.1016/j.powtec.2017.10.035

Natural vanilla extract (NVE) and synthetic vanilla extract (SVE) were microencapsulated by spray-drying, using whey protein concentrate (WPC) as wall material. Physicochemical properties, volatility profile, vanillin concentration and antioxidant activity were evaluated by measuring total polyphenols, the inhibition of radical scavenging activity by DPPH, chain-breaking activity and reducing power. Both microparticles exhibited high vanillin retention and antioxidant activity during spray dried process, but microparticles of SVE-WPC showed higher vanillin retention than microparticles of NVE-WPC during storage. The micrographs of the microcapsules showed morphological characteristics that were ideal for ensuring stability and integrity during storage to different water activities. WPC was found a suitable wall material to produce powder with vanilla extracts. Vanilla powder represents an interesting food additive for incorporation into functional foods. [Display omitted] •WPC is an alternative to produce powder with vanilla extract.•Vanillin was successfully microencapsulated using spray drying.•Microcapsules presented good physicochemical and antioxidant properties.•Microcapsules were not altered during storage period.•Natural and synthetic vanilla extracts produced powder with similar properties.