Utilizing the SIMS technique in the study of grain boundary diffusion along twist grain boundaries in the Cu(Ni) system
The secondary ion mass spectrometry (SIMS) technique was used to study grain boundary diffusion along (100) twist grain boundaries in the Cu(Ni) system. Concentration profiles of Ni down Cu twist grain boundaries with nominal disorientation angles of 10°, Σ5 (36.87°), and 45°, were measured using th...
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Published in | Acta materialia Vol. 50; no. 20; pp. 5079 - 5084 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Oxford
Elsevier Ltd
03.12.2002
Elsevier Science |
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Abstract | The secondary ion mass spectrometry (SIMS) technique was used to study grain boundary diffusion along (100) twist grain boundaries in the Cu(Ni) system. Concentration profiles of Ni down Cu twist grain boundaries with nominal disorientation angles of 10°,
Σ5 (36.87°), and 45°, were measured using the SIMS technique. The average activation energy for grain boundary diffusion,
Q
b, was found to be 245±22, 140±10, and 102±15 kJ/mol, for the 10°,
Σ5, and 45° twist grain boundaries, respectively. The average grain boundary diffusion pre-exponential term, s
δD
bo, was found to be 9.6±1.24×10
−9, 1.1±0.17×10
−14, and
1.3±0.36×10
−16
m
3
/s,
for the 10°,
Σ5, and 45° twist grain boundaries, respectively. |
---|---|
AbstractList | The secondary ion mass spectrometry (SIMS) technique was used to study grain boundary diffusion along (100) twist grain boundaries in the Cu(Ni) system. Concentration profiles of Ni down Cu twist grain boundaries with nominal disorientation angles of 10 deg , Sigma 5 (36.87 deg ), and 45 deg , were measured using the SIMS technique. The average activation energy for grain boundary diffusion, Q sub b , was found to be 245 plus/minus 22, 140 plus /minus 10, and 102 plus/minus 15 kJ/mol, for the 10 deg , Sigma 5, and 45 deg twist grain boundaries, respectively. The average grain boundary diffusion pre-exponential term, s delta D sub bo , was found to be 9.6 plus/minus 1.24 x 10 exp -9 , 1.1 plus/minus 0.17 x 10 exp -14 , and 1.3 plus/minus 0.36 x 10 exp -16 m exp 3 /s, for the 10 deg , Sigma 5, and 45 deg twist grain boundaries, respectively. The secondary ion mass spectrometry (SIMS) technique was used to study grain boundary diffusion along (100) twist grain boundaries in the Cu(Ni) system. Concentration profiles of Ni down Cu twist grain boundaries with nominal disorientation angles of 10°, Σ5 (36.87°), and 45°, were measured using the SIMS technique. The average activation energy for grain boundary diffusion, Q b, was found to be 245±22, 140±10, and 102±15 kJ/mol, for the 10°, Σ5, and 45° twist grain boundaries, respectively. The average grain boundary diffusion pre-exponential term, s δD bo, was found to be 9.6±1.24×10 −9, 1.1±0.17×10 −14, and 1.3±0.36×10 −16 m 3 /s, for the 10°, Σ5, and 45° twist grain boundaries, respectively. |
Author | Stevie, F.A. Giannuzzi, L.A. Kempshall, B.W. Schwarz, S.M. |
Author_xml | – sequence: 1 givenname: S.M. surname: Schwarz fullname: Schwarz, S.M. email: smschwarz@yahoo.com organization: Mechanical, Materials & Aerospace Engineering, University of Central Florida, 32816 Orlando, FL, USA – sequence: 2 givenname: B.W. surname: Kempshall fullname: Kempshall, B.W. organization: Mechanical, Materials & Aerospace Engineering, University of Central Florida, 32816 Orlando, FL, USA – sequence: 3 givenname: L.A. surname: Giannuzzi fullname: Giannuzzi, L.A. organization: Mechanical, Materials & Aerospace Engineering, University of Central Florida, 32816 Orlando, FL, USA – sequence: 4 givenname: F.A. surname: Stevie fullname: Stevie, F.A. organization: Analytical Instrumentation Facility, North Carolina State University, 27695 Raleigh, NC, USA |
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Keywords | Cu(Ni) SIMS Grain boundary diffusion Twist grain boundaries Grain boundaries Crystal defects Tilt boundaries Binary systems Nickel Copper Experimental study |
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References | Kaur, Mishin, Gust (BIB1) 1995 Sutton, Balluffi (BIB14) 1995 Brandon (BIB13) 1966; 14 Yukawa, Sinnott (BIB6) 1955; 203 Wilson, Stevie, Magee (BIB11) 1989 Gust, Hintz, Lodding, Odelius, Predel (BIB9) 1982; 30 Renouf (BIB5) 1970; 22 Krishtal, Shcherbakov, Mokrov, Markova (BIB2) 1970; 29 Shewmon (BIB7) 1998 Dorner, Gust, Hintz, Lodding, Odelius, Predel (BIB10) 1980; 28 Gust, Hintz, Lodding, Lučić, Odelius, Predel, Roll (BIB8) 1985; C4 Austin, Richard (BIB15) 1961; 32 Bernardini, Cabane (BIB3) 1973; 21 Aljeshin, Prokofjev (BIB4) 1986; 9 Schwarz, Houge, Giannuzzi, King (BIB12) 2001; 222 |
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SubjectTerms | Applied sciences Condensed matter: structure, mechanical and thermal properties Cu(Ni) Defects and impurities in crystals; microstructure Exact sciences and technology Grain and twin boundaries Grain boundary diffusion Metals. Metallurgy Physics SIMS Structure of solids and liquids; crystallography Twist grain boundaries |
Title | Utilizing the SIMS technique in the study of grain boundary diffusion along twist grain boundaries in the Cu(Ni) system |
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