Hierarchical porous carbons with controlled micropores and mesopores for supercapacitor electrode materials

Various porous carbons were prepared by CO 2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were characterized by using X-ray diffraction, transmission electron microscopy and nitrogen sorption at 77 K. The effects of CO 2 treatment on the...

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Published in	Carbon (New York) Vol. 46; no. 13; pp. 1718 - 1726
Main Authors	Xia, Kaisheng, Gao, Qiuming, Jiang, Jinhua, Hu, Juan
Format	Journal Article
Language	English
Published	Oxford Elsevier Ltd 01.11.2008 Elsevier Science
Subjects	Chemistry Colloidal state and disperse state Cross-disciplinary physics: materials science; rheology Electrochemistry Exact sciences and technology Fullerenes and related materials; diamonds, graphite General and physical chemistry Materials science Physics Porous materials Specific materials Surface physical chemistry Potassium hydroxide Micropore Pore structure Porous materials Activation XRD Nitrogen Carbon Precursor Mesoporosity Electrodes Sorption Microporosity Transmission electron microscopy Adsorption Pore Electrochemistry Capacitance Electrolytes Surface area
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Abstract	Various porous carbons were prepared by CO 2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were characterized by using X-ray diffraction, transmission electron microscopy and nitrogen sorption at 77 K. The effects of CO 2 treatment on their pore structures were discussed. Compared to the pristine mesoporous carbons, the samples subjected to CO 2 treatment exhibited remarkable improvement in textural properties. The electrochemical measurement in 6 M KOH electrolyte showed that CO 2 activation leads to better capacitive performances. The carbon CS15A6, which was obtained after CO 2 treatment for 6 h at 950 °C using CMK-3 as the precursor, showed the best electrochemical behavior with a specific gravimetric capacitance of 223 F/g and volumetric capacitance of 54 F/cm 3 at a scan rate of 2 mV/s and 73% retained ratio at 50 mV/s. The good capacitive behavior of CS15A6 may be attributed to the hierarchical pore structure (abundant micropores and interconnected mesopores with the size of 3–4 nm), high surface area (2749 m 2/g), large pore volume (2.09 cm 3/g), as well as well-balanced microporosity and mesoporosity.
AbstractList	Various porous carbons were prepared by CO2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were characterized by using X-ray diffraction, transmission electron microscopy and nitrogen sorption at 77 K. The effects of CO2 treatment on their pore structures were discussed. Compared to the pristine mesoporous carbons, the samples subjected to CO2 treatment exhibited remarkable improvement in textural properties. The electrochemical measurement in 6 M KOH electrolyte showed that CO2 activation leads to better capacitive performances. The carbon CS15A6, which was obtained after CO2 treatment for 6 h at 950 deg C using CMK-3 as the precursor, showed the best electrochemical behavior with a specific gravimetric capacitance of 223 F/g and volumetric capacitance of 54 F/cm3 at a scan rate of 2 mV/s and 73% retained ratio at 50 mV/s. The good capacitive behavior of CS15A6 may be attributed to the hierarchical pore structure (abundant micropores and interconnected mesopores with the size of 3-4 nm), high surface area (2749 m2/g), large pore volume (2.09 cm3/g), as well as well-balanced microporosity and mesoporosity. Various porous carbons were prepared by CO 2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were characterized by using X-ray diffraction, transmission electron microscopy and nitrogen sorption at 77 K. The effects of CO 2 treatment on their pore structures were discussed. Compared to the pristine mesoporous carbons, the samples subjected to CO 2 treatment exhibited remarkable improvement in textural properties. The electrochemical measurement in 6 M KOH electrolyte showed that CO 2 activation leads to better capacitive performances. The carbon CS15A6, which was obtained after CO 2 treatment for 6 h at 950 °C using CMK-3 as the precursor, showed the best electrochemical behavior with a specific gravimetric capacitance of 223 F/g and volumetric capacitance of 54 F/cm 3 at a scan rate of 2 mV/s and 73% retained ratio at 50 mV/s. The good capacitive behavior of CS15A6 may be attributed to the hierarchical pore structure (abundant micropores and interconnected mesopores with the size of 3–4 nm), high surface area (2749 m 2/g), large pore volume (2.09 cm 3/g), as well as well-balanced microporosity and mesoporosity.
Author	Hu, Juan Xia, Kaisheng Jiang, Jinhua Gao, Qiuming
Author_xml	– sequence: 1 givenname: Kaisheng surname: Xia fullname: Xia, Kaisheng – sequence: 2 givenname: Qiuming surname: Gao fullname: Gao, Qiuming email: qmgao@mail.sic.ac.cn – sequence: 3 givenname: Jinhua surname: Jiang fullname: Jiang, Jinhua – sequence: 4 givenname: Juan surname: Hu fullname: Hu, Juan
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Snippet	Various porous carbons were prepared by CO 2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were... Various porous carbons were prepared by CO2 activation of ordered mesoporous carbons and used as electrode materials for supercapacitor. The structures were...
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SubjectTerms	Chemistry Colloidal state and disperse state Cross-disciplinary physics: materials science; rheology Electrochemistry Exact sciences and technology Fullerenes and related materials; diamonds, graphite General and physical chemistry Materials science Physics Porous materials Specific materials Surface physical chemistry
Title	Hierarchical porous carbons with controlled micropores and mesopores for supercapacitor electrode materials
URI	https://dx.doi.org/10.1016/j.carbon.2008.07.018 https://www.proquest.com/docview/35385006
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