Photocatalytic hydroxylation of arylboronic acids using continuous flow reactors

The photocatalytic oxidation of mono- and di-substituted arylboronic acids to phenols has been investigated using a continuous flow photoreactor fitted with white LEDs. An EtOH–H 2 O solvent system accelerated conversion at 2 MPa; whereas reactions at atmospheric pressure allowed for moderately effi...

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Published inRSC advances Vol. 5; no. 9; pp. 6501 - 6504
Main Authors Penders, Inès G. T. M., Amara, Zacharias, Horvath, Raphael, Rossen, Kai, Poliakoff, Martyn, George, Michael W.
Format Journal Article
LanguageEnglish
Published 01.01.2015
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Summary:The photocatalytic oxidation of mono- and di-substituted arylboronic acids to phenols has been investigated using a continuous flow photoreactor fitted with white LEDs. An EtOH–H 2 O solvent system accelerated conversion at 2 MPa; whereas reactions at atmospheric pressure allowed for moderately efficient desymmetrisation.
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ISSN:2046-2069
2046-2069
DOI:10.1039/C4RA15588B