Uniaxial compression of metallurgical coke samples with progressive loading

• Published in: Fuel (Guildford) Vol. 226; pp. 163 - 171
• Main Authors: Jenkins, David R., Lomas, Hannah, Mahoney, Merrick
• Format: Journal Article
• Language: English
• Published: Kidlington Elsevier Ltd 15.08.2018; Elsevier BV
• Subjects: Breaking; Carbon; Coke; Compression; Compressive loading; Computed tomography; Image resolution; Load; Load bearing components; Measurement; Metallurgical coke; Metallurgy; Micro-CT; Microstructure; Plastic deformation; Stiffening; Compressive loading; Micro-CT; Metallurgical coke
• ISSN: 0016-2361; 1873-7153
• DOI: 10.1016/j.fuel.2018.03.173

•Coke samples show stiffening at low compressive loads.•Stiffening presumably due to closing of fine scale porosity and re-arrangement of graphitic layers.•Damage at higher loads due to breakage of small load-bearing microstructure components.•Determination of plastic strain show these changes permanently alter the material under load. Coke samples, produced from coals having a range of rank and vitrinite content, were subjected to uniaxial loading in a universal tester. Cokes were also imaged at high resolution using micro-CT. The aim was to understand the relationship between the internal microstructure of the coke and coke strength under load. The loading was done in two separate ways, being either compression to failure or progressive loading. The results showed that the coke samples underwent a form of stiffening at low loads, potentially due to closing of fine-scale pores and/or re-alignment of graphitic layers in the RMDC. Measurements of plastic strain indicated that these changes were permanent. At higher loads, small load-bearing components of the microstructure were found to break, leading to a softening of the coke samples. Evidence of the breaking was observed using micro-CT images before and after loading of samples. The work has relevance to the understanding of the fundamentals of coke strength, as well as to issues relating to handling and preparation of coke for standard testing.