Reaction of 1, 1-(2, 2'-Oxydiethyl) biguanide with Dicyanodiamide

Thermal reaction of equimolar amounts of 1, 1-(2, 2'-oxydiethyl) biguanide with dicyanodiamide afforded a compound (I) other than the both reactants. The analytical data, infrared spectra, and chemical properties of I agreeded closely with those of 2-morpho-lino-4, 6-diamino-s-triazine, synthes...

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Published inChemical & pharmaceutical bulletin Vol. 12; no. 4; pp. 497 - 499
Main Authors Ueda, Takeo, Takahashi, Kiyoshi, Kobayashi, Sachiko
Format Journal Article
LanguageEnglish
Published Japan The Pharmaceutical Society of Japan 01.04.1964
Japan Science and Technology Agency
Subjects
Amides
Anesthetics, Local
Antiviral Agents
Biguanides
Chemistry, Pharmaceutical
Cyanides
Guanidine
Guanidines
Morpholines
Old Medline
ANTIVIRAL AGENTS
CHEMISTRY, PHARMACEUTICAL
GUANIDINES
MORPHOLINES
EXPERIMENTAL LAB STUDY
CYANIDES
AMIDES
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Summary:Thermal reaction of equimolar amounts of 1, 1-(2, 2'-oxydiethyl) biguanide with dicyanodiamide afforded a compound (I) other than the both reactants. The analytical data, infrared spectra, and chemical properties of I agreeded closely with those of 2-morpho-lino-4, 6-diamino-s-triazine, synthesized by conventional manner from cyanuric chloride, ammonia, and morpholine. Consequently, I was verified to be 2-morpholino-4, 6-diamino-s-triazine.
Bibliography:ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
ISSN:0009-2363
1347-5223
DOI:10.1248/cpb.12.497