Operando Neutron Scattering: Following Reactions in Real Time Using Neutrons

The complexation of NiCl 2 with 2,2′-Bipyridine was followed using quasielastic neutron scattering to observe reaction progress. Water adsorption in chabazite with time resolution was observed using strain induced in the aluminosilicate framework with a high-resolution engineering diffractometer. Th...

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Bibliographic Details
Published inTopics in catalysis Vol. 64; no. 9-12; pp. 693 - 698
Main Authors Skukauskas, Vainius, Johnson Humphrey, Elliot L. B., Hitchcock, Iain, York, Andrew, Kelleher, Joseph, Gibson, Emma K., Nelson, David J., Silverwood, Ian P.
Format Journal Article
LanguageEnglish
Published New York Springer US 01.08.2021
Springer Nature B.V
Subjects
Adsorbed water
Aluminosilicates
Aluminum silicates
Catalysis
Characterization and Evaluation of Materials
Chemistry
Chemistry and Materials Science
Industrial Chemistry/Chemical Engineering
Neutron scattering
Neutrons
Original Paper
Pharmacy
Physical Chemistry
Operando
Catalysis
Quasielastic neutron scattering
QENS
Neutron diffraction
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Summary:The complexation of NiCl 2 with 2,2′-Bipyridine was followed using quasielastic neutron scattering to observe reaction progress. Water adsorption in chabazite with time resolution was observed using strain induced in the aluminosilicate framework with a high-resolution engineering diffractometer. These reactions illustrate the recent progress and possibilities in using neutron probes to observe realistic catalytic reactions as they progress.
ISSN:1022-5528
1572-9028
DOI:10.1007/s11244-021-01436-x