A NEW SYNTHESIS OF 3H-CYCL[3.2.2]AZINO[1,2-E]CYCL[3.3.2]-AZIN-3-ONE DERIVATIVE

Treatment of indolizinoquinolizinium salt (6) with dimethyl acetylenedicarboxylate in the presence of K2CO3 in refluxing nitrobenzene gave a nitrogen-bridged annulenoannulenone, 3H-cycl[3.2.2]azino[1,2-e]cycl[3.3.2]azinone derivative (7).

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Bibliographic Details
Published inHeterocycles Vol. 34; no. 12; pp. 2277 - 2280
Main Authors MATSUDA, Y, GOTOU, H, YAMASHITA, M, TAKAHASHI, K, IDE, S, FURUNO, K, TORISU, K, ITOU, T, MOTOKAWA, C
Format Journal Article
LanguageEnglish
Published OXFORD Elsevier 01.12.1992
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Summary:Treatment of indolizinoquinolizinium salt (6) with dimethyl acetylenedicarboxylate in the presence of K2CO3 in refluxing nitrobenzene gave a nitrogen-bridged annulenoannulenone, 3H-cycl[3.2.2]azino[1,2-e]cycl[3.3.2]azinone derivative (7).
ISSN:0385-5414
DOI:10.3987/COM-92-6174