Determination of Dihydrobenzoacridinone Structures by NMR, IR, and UV Spectroscopy and Mass Spectrometry

Condensation of 2-naphthylamine, aromatic aldehydes, and dimedone was found to produce 9,10-dihydrobenzo[a] acridin-11-one derivatives according to PMR, 13 C NMR, and IR spectroscopy and mass spectrometry. Correlation spectroscopy showed that the carbonyl in the synthesized dihydrobenzoacridinone de...

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Bibliographic Details
Published inJournal of applied spectroscopy Vol. 82; no. 6; pp. 915 - 919
Main Authors Kozlov, N. G., Zhiharko, Yu. D., Skakovsky, E. D., Baranovsky, A. V., Ogorodnikova, M. M., Basalaeva, L. I.
Format Journal Article
LanguageEnglish
Published New York Springer US 2016
Springer
Subjects
Aldehydes
Analytical Chemistry
Atomic/Molecular Structure and Spectra
Mass spectrometry
Nuclear magnetic resonance spectroscopy
Physics
Physics and Astronomy
three-component condensation
2-naphthylamine
spectroscopy
dihydrobenzoacridinones
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Summary:Condensation of 2-naphthylamine, aromatic aldehydes, and dimedone was found to produce 9,10-dihydrobenzo[a] acridin-11-one derivatives according to PMR, 13 C NMR, and IR spectroscopy and mass spectrometry. Correlation spectroscopy showed that the carbonyl in the synthesized dihydrobenzoacridinone derivatives was located on C 11 .
ISSN:0021-9037
1573-8647
DOI:10.1007/s10812-016-0204-6