Effect of Nb and Si Content on Phase Stability, Microstructure and Mechanical Properties of Sintered Ti–Nb–Si Alloys

The development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This approach aims to enhance biocompatibility and mitigate potential cytotoxic effects associated with traditional alloying elements. In this work...

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Published inMetals (Basel ) Vol. 15; no. 1; p. 34
Main Authors Luup Carvalho, Derek Manoel, Paim, Deivison Daros, Schramm Deschamps, Isadora, Aguilar, Claudio, Klein, Aloísio Nelmo, Cavilha Neto, Francisco, Oliveira Neves, Guilherme, Binder, Cristiano
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 01.01.2025
Subjects
Alloying elements
Beta phase
Biocompatibility
biomaterials
Cold pressing
Corrosion resistance
Design of experiments
elastic modulus
Energy consumption
Grains
Industrial development
Mechanical properties
Metal products
Niobium base alloys
Phase stability
Powder metallurgy
Powders
Precipitates
Precipitation heat treatment
Silicon
Sintering
Sintering (powder metallurgy)
Specialty metals industry
Specific gravity
thermodynamics
Titanium
Titanium alloys
Titanium base alloys
Transplants & implants
Ultimate tensile strength
Wear resistance
Yield stress
Canada
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Abstract The development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This approach aims to enhance biocompatibility and mitigate potential cytotoxic effects associated with traditional alloying elements. In this work, Ti–xNb–ySi alloys were produced using powder metallurgy, with x of 35, 40, and 45 wt.%, and y of 0.10, 0.35, and 0.60% wt.%, using a 32 experimental design. Milling was used to mix and disperse the powders, followed by cold pressing, sintering, and heat treatment. Nb was the main element used to stabilize the β phase, and Si was used to form Si precipitates, although Si also exhibits a β-stabilizing effect. It was found that an increase from 0.10 to 0.35 wt.% of Si improved relative density, with no benefits observed at 0.60 wt.% Si. Electron microscopy showed the presence of β phase grains, and grains with β + α intragranular structures and precipitates. Increasing Nb content resulted in a decrease in ultimate tensile strength while increasing Si content from 0.10% to 0.35 wt.% exhibited the opposite effect.
AbstractList AbstractThe development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This approach aims to enhance biocompatibility and mitigate potential cytotoxic effects associated with traditional alloying elements. In this work, Ti–xNb–ySi alloys were produced using powder metallurgy, with x of 35, 40, and 45 wt.%, and y of 0.10, 0.35, and 0.60% wt.%, using a 32 experimental design. Milling was used to mix and disperse the powders, followed by cold pressing, sintering, and heat treatment. Nb was the main element used to stabilize the β phase, and Si was used to form Si precipitates, although Si also exhibits a β-stabilizing effect. It was found that an increase from 0.10 to 0.35 wt.% of Si improved relative density, with no benefits observed at 0.60 wt.% Si. Electron microscopy showed the presence of β phase grains, and grains with β + α intragranular structures and precipitates. Increasing Nb content resulted in a decrease in ultimate tensile strength while increasing Si content from 0.10% to 0.35 wt.% exhibited the opposite effect.
The development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This approach aims to enhance biocompatibility and mitigate potential cytotoxic effects associated with traditional alloying elements. In this work, Ti–xNb–ySi alloys were produced using powder metallurgy, with x of 35, 40, and 45 wt.%, and y of 0.10, 0.35, and 0.60% wt.%, using a 32 experimental design. Milling was used to mix and disperse the powders, followed by cold pressing, sintering, and heat treatment. Nb was the main element used to stabilize the β phase, and Si was used to form Si precipitates, although Si also exhibits a β-stabilizing effect. It was found that an increase from 0.10 to 0.35 wt.% of Si improved relative density, with no benefits observed at 0.60 wt.% Si. Electron microscopy showed the presence of β phase grains, and grains with β + α intragranular structures and precipitates. Increasing Nb content resulted in a decrease in ultimate tensile strength while increasing Si content from 0.10% to 0.35 wt.% exhibited the opposite effect.
The development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This approach aims to enhance biocompatibility and mitigate potential cytotoxic effects associated with traditional alloying elements. In this work, Ti–xNb–ySi alloys were produced using powder metallurgy, with x of 35, 40, and 45 wt.%, and y of 0.10, 0.35, and 0.60% wt.%, using a 3[sup.2] experimental design. Milling was used to mix and disperse the powders, followed by cold pressing, sintering, and heat treatment. Nb was the main element used to stabilize the β phase, and Si was used to form Si precipitates, although Si also exhibits a β-stabilizing effect. It was found that an increase from 0.10 to 0.35 wt.% of Si improved relative density, with no benefits observed at 0.60 wt.% Si. Electron microscopy showed the presence of β phase grains, and grains with β + α intragranular structures and precipitates. Increasing Nb content resulted in a decrease in ultimate tensile strength while increasing Si content from 0.10% to 0.35 wt.% exhibited the opposite effect.
Audience Academic
Author Schramm Deschamps, Isadora
Binder, Cristiano
Oliveira Neves, Guilherme
Paim, Deivison Daros
Klein, Aloísio Nelmo
Cavilha Neto, Francisco
Luup Carvalho, Derek Manoel
Aguilar, Claudio
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Snippet The development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical industry. This...
AbstractThe development of beta titanium alloys with biocompatible elements to replace Al and V is a subject of significant interest in the biomedical...
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SubjectTerms Alloying elements
Beta phase
Biocompatibility
biomaterials
Cold pressing
Corrosion resistance
Design of experiments
elastic modulus
Energy consumption
Grains
Industrial development
Mechanical properties
Metal products
Niobium base alloys
Phase stability
Powder metallurgy
Powders
Precipitates
Precipitation heat treatment
Silicon
Sintering
Sintering (powder metallurgy)
Specialty metals industry
Specific gravity
thermodynamics
Titanium
Titanium alloys
Titanium base alloys
Transplants & implants
Ultimate tensile strength
Wear resistance
Yield stress
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Title Effect of Nb and Si Content on Phase Stability, Microstructure and Mechanical Properties of Sintered Ti–Nb–Si Alloys
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