A Microwave-Assisted Heck Reaction in Poly(ethylene glycol) for the Synthesis of Benzazepines

The Heck reaction of alkylated 2‐(trimethylsilyl)ethanesulfonyl (SES)‐protected β‐amino esters provides benzazepines in good yields. Good selectivity towards cyclisation was obtained when the reaction was performed in PEG 3400 as the solvent under microwave activation. Cleavage of the SES group with...

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Bibliographic Details
Published inEuropean Journal of Organic Chemistry Vol. 2007; no. 1; pp. 201 - 208
Main Authors Declerck, Valérie, Ribière, Patrice, Nédellec, Yannig, Allouchi, Hassan, Martinez, Jean, Lamaty, Frédéric
Format Book Review Journal Article
LanguageEnglish
Published Weinheim WILEY-VCH Verlag 01.01.2007
WILEY‐VCH Verlag
Wiley
Wiley-VCH Verlag
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