Effects of chemical segregation on ductility-anisotropy in high strength Fe-Mn-Al-C lightweight austenitic steels

• Published in: Acta materialia Vol. 245; p. 118589
• Main Authors: Picak, S., Vaughan, M.W., Atwani, O. El, Mott, A., Limmer, K.R., Karaman, I.
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 15.02.2023
• Subjects: Chemical segregation; Fe-Mn-Al-C; Low density steels; Precipitation hardening; Ultra-high strength steels; Fe-Mn-Al-C; Chemical segregation; Low density steels; Ultra-high strength steels; Precipitation hardening
• ISSN: 1359-6454; 1873-2453
• DOI: 10.1016/j.actamat.2022.118589

Ductile Fe-Mn-Al-C lightweight steels offer great potential as high specific strength materials for weight critical applications. In the present work, very high yield (∼1 GPa) and ultimate tensile strength levels (∼1.5 GPa) were obtained along the rolling and transverse directions of Fe-30Mn-8.5Al-0.9Si-0.9C-0.5Mo (wt.%), with high tensile elongation to failure of ∼35%. This excellent mechanical behavior was attributed to the nanoscale, ordered κ-carbide precipitates formed during aging after rolling. However, tensile ductility was not isotropic through all directions of the rolled plate. In particular, the ductility was consistently lower than 5% true strain along the normal direction. Upon detailed microstructural investigations, micro-scale lamellar chemical micro-segregation bands were detected, which caused the observed anisotropic embrittlement along certain plate directions. These bands resulted in low failure strains along the normal direction since it is oriented perpendicular to these chemical segregation bands, resulting in a failure type reminiscent of delamination-induced cleavage fracture. Chemical segregation causes an inhomogeneous κ-carbide precipitate distribution upon aging, producing more pronounced mechanical anisotropy after peak-aging as compared to the solution heat treated samples. Surprisingly, deformation twinning was observed after tensile deformation of solution-heat treated specimens via electron-backscatter diffraction experiments, which is anomalous for a high stacking fault energy (SFE) material. It was proposed that chemical micro-segregation promotes locally different SFE regions, leading to deformation twinning in this nominally high SFE material. Overall, this work demonstrates the effects of chemical segregation on mechanical properties and microstructural evolution in a high performance, lightweight Fe-Mn-Al-C steel. [Display omitted]