4-Hydroxy-3-methoxybenzaldehyde 4-phenylthiosemicarbazone

In the title compound, C 15 H 15 N 3 O 2 S, the central C—N—N—C unit has an anti conformation [torsion angle = −170.17 (15)°]. The phenyl substituent is oriented perpendicular to this unit [dihedral angle of 89.2 (1)°], whereas the substituted ring is rotated out of this plane by only 18.86 (17)°. I...

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Bibliographic Details
Published inActa crystallographica. Section E, Structure reports online Vol. 70; no. 3; p. o278
Main Authors Oliveira, Adriano Bof de, Feitosa, Bárbara Regina Santos, Näther, Christian, Jess, Inke
Format Journal Article
LanguageEnglish
Published International Union of Crystallography 01.03.2014
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Summary:In the title compound, C 15 H 15 N 3 O 2 S, the central C—N—N—C unit has an anti conformation [torsion angle = −170.17 (15)°]. The phenyl substituent is oriented perpendicular to this unit [dihedral angle of 89.2 (1)°], whereas the substituted ring is rotated out of this plane by only 18.86 (17)°. In the crystal, molecules are linked by pairs of N—H...S hydrogen bonds into inversion dimers that are further connected via N—H...O and O—H...S hydrogen bonds into a three-dimensional network.
ISSN:1600-5368
1600-5368
DOI:10.1107/S1600536814002773