Synthesis and physicochemical study of nonamolybdomanganate with the hexamminecadmium cation

Hexamminecadmium nonamolybdomanganate [Cd(NH 3 ) 6 ] · H 4 [MnMo 9 O 32 ] · 6H 2 O was prepared and studied by mass spectrometry, thermogravimetry, powder X-ray diffraction, and IR spectroscopy. The crystals are monoclinic: a = 14.81 Å, b = 14.82 Å, c = 14.23 Å, β = 119.04°, V = 2703.70 Å 3 , ρ calc...

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Published inRussian journal of inorganic chemistry Vol. 58; no. 5; pp. 512 - 514
Main Authors Oreshkina, A. V., Kaziev, G. Z., Steblevskii, A. V., Holguin Quinones, S., Peretokina, O. N., de Ita, A.
Format Journal Article
LanguageEnglish
Published Dordrecht SP MAIK Nauka/Interperiodica 01.05.2013
Subjects
Cations
Chemistry
Chemistry and Materials Science
Crystals
Diffraction
Infrared radiation
Inorganic Chemistry
Mass spectrometry
Synthesis
Synthesis and Properties of Inorganic Compounds
Thermogravimetry
X-rays
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Summary:Hexamminecadmium nonamolybdomanganate [Cd(NH 3 ) 6 ] · H 4 [MnMo 9 O 32 ] · 6H 2 O was prepared and studied by mass spectrometry, thermogravimetry, powder X-ray diffraction, and IR spectroscopy. The crystals are monoclinic: a = 14.81 Å, b = 14.82 Å, c = 14.23 Å, β = 119.04°, V = 2703.70 Å 3 , ρ calc = 3.23 g/cm 3 , Z = 3.
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ISSN:0036-0236
1531-8613
DOI:10.1134/S0036023613050161