Microwave-assisted benzyl-transfer reactions of commercially available 2-benzyloxy-1-methylpyridinium triflate

Benzylation of alcohols and other substrates under thermal conditions translates smoothly from conventional heating into MW-assisted organic synthesis(MAOS). Reactions times are decreased from hours to minutes while good to excellent yields are maintained. MW heating should be considered for benzyla...

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Published inOrganic & biomolecular chemistry Vol. 10; no. 2; pp. 248 - 250
Main Authors Wang, Teng-wei, Intaranukulkit, Tanit, Rosana, Michael R., Slegeris, Rimantas, Simon, Janet, Dudley, Gregory B.
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 14.01.2012
Subjects
Alcohols - chemistry
Benzyl Compounds - chemistry
Carboxylic Acids - chemistry
Chemistry
Chemistry, Organic
Ethers - chemical synthesis
Ethers - chemistry
Mesylates - chemistry
Microwaves
Molecular Structure
Physical Sciences
Pyridinium Compounds - chemistry
Science & Technology
ALCOHOLS
SALT
DERIVATIVES
ESTERS
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Summary:Benzylation of alcohols and other substrates under thermal conditions translates smoothly from conventional heating into MW-assisted organic synthesis(MAOS). Reactions times are decreased from hours to minutes while good to excellent yields are maintained. MW heating should be considered for benzylation of high-value substrates using the title reagent.
Bibliography:ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
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ISSN:1477-0520
1477-0539
DOI:10.1039/c1ob06504a