Higher-order polysulfides induced thermal runaway for 1.0 Ah lithium sulfur pouch cells
Comprehensive analyses on thermal runaway mechanisms are critically vital to achieve the safe lithium–sulfur (Li–S) batteries. The reactions between dissolved higher-order polysulfides and Li metal were found to be the origins for the thermal runaway of 1.0 Ah cycled Li–S pouch cells. 16-cycle pouch...
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| Published in | Particuology Vol. 79; pp. 10 - 17 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.08.2023
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| Abstract | Comprehensive analyses on thermal runaway mechanisms are critically vital to achieve the safe lithium–sulfur (Li–S) batteries. The reactions between dissolved higher-order polysulfides and Li metal were found to be the origins for the thermal runaway of 1.0 Ah cycled Li–S pouch cells. 16-cycle pouch cell indicates high safety, heating from 30 to 300 °C without thermal runaway, while 16-cycle pouch cell with additional electrolyte undergoes severe thermal runaway at 147.9 °C, demonstrating the key roles of the electrolyte on the thermal safety of batteries. On the contrary, thermal runaway does not occur for 45-cycle pouch cell despite the addition of the electrolyte. It is found that the higher-order polysulfides (Li2Sx ≥ 6) are discovered in 16-cycle electrolyte while the sulfur species in 45-cycle electrolyte are Li2Sx ≤ 4. In addition, strong exothermic reactions are discovered between cycled Li and dissolved higher-order polysulfide (Li2S6 and Li2S8) at 153.0 °C, driving the thermal runaway of cycled Li–S pouch cells. This work uncovers the potential safety risks of Li–S batteries and negative roles of the polysulfide shuttle for Li–S batteries from the safety view.
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•The thermal safety of deeply cycled Li–S pouch cells have been systematically investigated.•Thermal behaviors of 16-cycle cells with/without electrolytes are due to different viscosities.•The thermal safety of 16/45-cycle cells depends on the polysulfides species in electrolytes. |
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| AbstractList | Comprehensive analyses on thermal runaway mechanisms are critically vital to achieve the safe lithium–sulfur (Li–S) batteries. The reactions between dissolved higher-order polysulfides and Li metal were found to be the origins for the thermal runaway of 1.0 Ah cycled Li–S pouch cells. 16-cycle pouch cell indicates high safety, heating from 30 to 300 °C without thermal runaway, while 16-cycle pouch cell with additional electrolyte undergoes severe thermal runaway at 147.9 °C, demonstrating the key roles of the electrolyte on the thermal safety of batteries. On the contrary, thermal runaway does not occur for 45-cycle pouch cell despite the addition of the electrolyte. It is found that the higher-order polysulfides (Li2Sx ≥ 6) are discovered in 16-cycle electrolyte while the sulfur species in 45-cycle electrolyte are Li2Sx ≤ 4. In addition, strong exothermic reactions are discovered between cycled Li and dissolved higher-order polysulfide (Li2S6 and Li2S8) at 153.0 °C, driving the thermal runaway of cycled Li–S pouch cells. This work uncovers the potential safety risks of Li–S batteries and negative roles of the polysulfide shuttle for Li–S batteries from the safety view.
[Display omitted]
•The thermal safety of deeply cycled Li–S pouch cells have been systematically investigated.•Thermal behaviors of 16-cycle cells with/without electrolytes are due to different viscosities.•The thermal safety of 16/45-cycle cells depends on the polysulfides species in electrolytes. |
| Author | Liu, He Chen, Zi-Xian Yuan, Hong Zhang, Qiang Yang, Shi-Jie Huang, Jia-Qi Liu, Lei Cheng, Xin-Bing Jiang, Feng-Ni |
| Author_xml | – sequence: 1 givenname: Feng-Ni surname: Jiang fullname: Jiang, Feng-Ni organization: College of Chemical Engineering and Technology, Taiyuan University of Technology, Taiyuan, 030024, Shanxi, China – sequence: 2 givenname: Shi-Jie surname: Yang fullname: Yang, Shi-Jie organization: Advanced Research Institute of Multidisciplinary Science, Beijing Institute of Technology, Beijing, 100081, China – sequence: 3 givenname: Zi-Xian surname: Chen fullname: Chen, Zi-Xian organization: Advanced Research Institute of Multidisciplinary Science, Beijing Institute of Technology, Beijing, 100081, China – sequence: 4 givenname: He surname: Liu fullname: Liu, He organization: Advanced Research Institute of Multidisciplinary Science, Beijing Institute of Technology, Beijing, 100081, China – sequence: 5 givenname: Hong surname: Yuan fullname: Yuan, Hong organization: Advanced Research Institute of Multidisciplinary Science, Beijing Institute of Technology, Beijing, 100081, China – sequence: 6 givenname: Lei surname: Liu fullname: Liu, Lei organization: College of Chemical Engineering and Technology, Taiyuan University of Technology, Taiyuan, 030024, Shanxi, China – sequence: 7 givenname: Jia-Qi surname: Huang fullname: Huang, Jia-Qi organization: Advanced Research Institute of Multidisciplinary Science, Beijing Institute of Technology, Beijing, 100081, China – sequence: 8 givenname: Xin-Bing orcidid: 0000-0001-7567-1210 surname: Cheng fullname: Cheng, Xin-Bing email: chengxb@seu.edu.cn organization: Key Laboratory of Energy Thermal Conversion and Control of Ministry of Education, School of Energy and Environment, Southeast University, Nanjing, 211189, Jiangsu, China – sequence: 9 givenname: Qiang surname: Zhang fullname: Zhang, Qiang organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering, Tsinghua University, Beijing, 100084, China |
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| Keywords | Polysulfides Lithium–sulfur batteries Pouch cell Polysulfide shuttle Thermal runaway |
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| Title | Higher-order polysulfides induced thermal runaway for 1.0 Ah lithium sulfur pouch cells |
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