AN EFFICIENT AND SIMPLE PROCEDURE FOR PREPARATION OF ESTERS AND ANHYDRIDES FROM ACID CHLORIDES IN THE PRESENCE OF 1,4-DIAZABICYCLO[2.2.2]OCTANE (DABCO) UNDER SOLVENT-FREE CONDITIONS

A manipulatively one-pot and rapid method for the synthesis of aliphatic and aromatic ester and anhydride from acid chloride and alcohol or potassium salt of carboxylic acid under solvent-free conditions is reported. The reaction has been carried out in excellent yield and short reaction time in the...

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Bibliographic Details
Published inSynthetic communications Vol. 32; no. 1; pp. 23 - 30
Main Authors Hajipour, A. R., Mazloumi, Gh
Format Journal Article
LanguageEnglish
Published NEW YORK Taylor & Francis Group 01.01.2002
Marcel Dekker Inc
Subjects
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
ALCOHOLS
OXIDATION
REAGENT
ORGANIC-SYNTHESIS
SOLID-STATE CONDITIONS
ACYLATION
CONVENIENT
MICROWAVE IRRADIATION
ALUMINA
TRANSESTERIFICATION
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Summary:A manipulatively one-pot and rapid method for the synthesis of aliphatic and aromatic ester and anhydride from acid chloride and alcohol or potassium salt of carboxylic acid under solvent-free conditions is reported. The reaction has been carried out in excellent yield and short reaction time in the presence of 1,4-diazabicyclo[2.2.2]octane (DABCO) under solvent-free conditions.
ISSN:0039-7911
1532-2432
DOI:10.1081/SCC-120001504