CuO/Cu composite nanospheres on a TiO2 nanotube array for amperometric sensing of glucose
A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a dia...
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| Published in | Mikrochimica acta (1966) Vol. 187; no. 2; p. 123 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Vienna
Springer Vienna
01.02.2020
Springer Nature B.V |
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| Abstract | A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a diameter of ~200 nm are well dispersed on the TNT surface, which warrants smooth interaction and a 3D nanostructure with high uniformity. The modified electrode was then used for amperometric determination of glucose in 0.1 M NaOH solution. Figures of merit include (a) a typical working voltage of 0.65 V (vs. Ag/AgCl). (b) a linear range as wide as from 0.2–90 mM, (c) good sensitivity (234 μA mM
−1
cm
−2
), and a 19 nM lower detection limit. The sensor is selective over ascorbic acid (AA), dopamine (DA), uric acid (UA), lactose, sucrose, and fructose.
Graphical abstract |
|---|---|
| AbstractList | A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a diameter of ~200 nm are well dispersed on the TNT surface, which warrants smooth interaction and a 3D nanostructure with high uniformity. The modified electrode was then used for amperometric determination of glucose in 0.1 M NaOH solution. Figures of merit include (a) a typical working voltage of 0.65 V (vs. Ag/AgCl). (b) a linear range as wide as from 0.2–90 mM, (c) good sensitivity (234 μA mM
−1
cm
−2
), and a 19 nM lower detection limit. The sensor is selective over ascorbic acid (AA), dopamine (DA), uric acid (UA), lactose, sucrose, and fructose.
Graphical abstract A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a diameter of ~200 nm are well dispersed on the TNT surface, which warrants smooth interaction and a 3D nanostructure with high uniformity. The modified electrode was then used for amperometric determination of glucose in 0.1 M NaOH solution. Figures of merit include (a) a typical working voltage of 0.65 V (vs. Ag/AgCl). (b) a linear range as wide as from 0.2-90 mM, (c) good sensitivity (234 μA mM-1 cm-2), and a 19 nM lower detection limit. The sensor is selective over ascorbic acid (AA), dopamine (DA), uric acid (UA), lactose, sucrose, and fructose. Graphical abstract.A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a diameter of ~200 nm are well dispersed on the TNT surface, which warrants smooth interaction and a 3D nanostructure with high uniformity. The modified electrode was then used for amperometric determination of glucose in 0.1 M NaOH solution. Figures of merit include (a) a typical working voltage of 0.65 V (vs. Ag/AgCl). (b) a linear range as wide as from 0.2-90 mM, (c) good sensitivity (234 μA mM-1 cm-2), and a 19 nM lower detection limit. The sensor is selective over ascorbic acid (AA), dopamine (DA), uric acid (UA), lactose, sucrose, and fructose. Graphical abstract. A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The electrode was fabricated by coating the CuO-Cu nanospheres onto the TNT array through electrochemical deposition. The CuO-Cu nanospheres with a diameter of ~200 nm are well dispersed on the TNT surface, which warrants smooth interaction and a 3D nanostructure with high uniformity. The modified electrode was then used for amperometric determination of glucose in 0.1 M NaOH solution. Figures of merit include (a) a typical working voltage of 0.65 V (vs. Ag/AgCl). (b) a linear range as wide as from 0.2–90 mM, (c) good sensitivity (234 μA mM−1 cm−2), and a 19 nM lower detection limit. The sensor is selective over ascorbic acid (AA), dopamine (DA), uric acid (UA), lactose, sucrose, and fructose. |
| ArticleNumber | 123 |
| Author | Shao, Jiahui Zhou, Zhiru Zhu, Zanzan Zhou, Hong Susan Cui, Feiyun |
| Author_xml | – sequence: 1 givenname: Zhiru surname: Zhou fullname: Zhou, Zhiru organization: Department of Chemical engineering, Worcester Polytechnic Institute – sequence: 2 givenname: Zanzan surname: Zhu fullname: Zhu, Zanzan organization: Department of Chemical engineering, Worcester Polytechnic Institute, National Cancer Centre Singapore – sequence: 3 givenname: Feiyun surname: Cui fullname: Cui, Feiyun organization: Department of Chemical engineering, Worcester Polytechnic Institute – sequence: 4 givenname: Jiahui surname: Shao fullname: Shao, Jiahui organization: School of Environmental Science and Engineering, Shanghai Jiao Tong University – sequence: 5 givenname: Hong Susan orcidid: 0000-0002-6659-6965 surname: Zhou fullname: Zhou, Hong Susan email: szhou@wpi.edu organization: Department of Chemical engineering, Worcester Polytechnic Institute |
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| Keywords | Wide analytical range Enzymeless sensing Glucose sensor Amperometric sensing nanotube arrays CuO-Cu nanospheres TiO |
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| Snippet | A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The... A non-enzymatic glucose sensor based on the use of CuO-Cu nanospheres placed on a TiO2 nanotube (TNT) array with excellent performance is described. The... |
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| SubjectTerms | Analytical Chemistry Ascorbic acid Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Coated electrodes Copper Copper oxides Dopamine Electrical measurement Electrodes Glucose Lactose Microengineering Nanochemistry Nanospheres Nanotechnology Nanotubes Original Paper Sensor arrays Silver chloride Sucrose Titanium dioxide Uric acid |
| Title | CuO/Cu composite nanospheres on a TiO2 nanotube array for amperometric sensing of glucose |
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