Study on Morphology and Crystal Structure of Pd Doped Nd1.2FeO3

Study on morphology and crystal structure of Nd1.2PdxFe1-xO3 doped Pd (1,2,3,4 and 5 wt%) synthesized by solid state reaction method have been investigated. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used to identify phase and morphology of sample. Further analysis using X’P...

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Bibliographic Details
Published inMaterials today : proceedings Vol. 13; pp. 258 - 263
Main Authors Sujiono, Eko Hadi, Zharvan, Vicran, Dahlan, Muhammad Yusriadi, Said, Andi Chaerunnisa Mugni, Agus, Jasdar, Samnur
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 2019
Subjects
crystal structure
crystalline size
morphology
NdFeO3
palladium
crystal structure
palladium
morphology
NdFeO3
crystalline size
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Summary:Study on morphology and crystal structure of Nd1.2PdxFe1-xO3 doped Pd (1,2,3,4 and 5 wt%) synthesized by solid state reaction method have been investigated. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used to identify phase and morphology of sample. Further analysis using X’Pert High Score Plus software show that samples have two phases: Nd1.2PdxFe1-xO3 as major phase and Nd2O3 as a minor phase. Nd1.2PdxFe1-xO3 crystalline size obtained by Scherrer equation has a value ranging from 43 to 50 nm and also has spherical shapes with the small existence of Pd confirmed by EDS results.
ISSN:2214-7853
2214-7853
DOI:10.1016/j.matpr.2019.03.224