Mechanically Activated Solid-State Synthesis of Flavones by High-Speed Ball Milling

An efficient, mechanically activated solid-state synthesis of flavones from 1-(2-hydroxyphenyl)-3-aryl-1,3-propanediones using high-speed ball milling is described. This method has notable advantages in terms of good yield, short reaction time, and neat conditions.

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Bibliographic Details
Published inSynthetic communications Vol. 39; no. 23; pp. 4199 - 4211
Main Authors Zhu, Xingyi, Li, Zhenhua, Shu, Qiangfeng, Zhou, Chenfeng, Su, Weike
Format Journal Article
LanguageEnglish
Published PHILADELPHIA Taylor & Francis Group 05.11.2009
Taylor & Francis
Subjects
Ball milling
Chemistry
Chemistry, Organic
flavones
Physical Sciences
Science & Technology
solid-state synthesis
OXIDATION
ACID
ONE-POT
Ball milling
solid-state synthesis
INDOLES
FLAVANONES
POTASSIUM HYDROGEN SULFATE
FACILE SYNTHESIS
flavones
KHSO4
EFFICIENT
SOLVENT-FREE SYNTHESIS
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Summary:An efficient, mechanically activated solid-state synthesis of flavones from 1-(2-hydroxyphenyl)-3-aryl-1,3-propanediones using high-speed ball milling is described. This method has notable advantages in terms of good yield, short reaction time, and neat conditions.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397910902898551