Deacetylation of Thioacetate using Acetyl Chloride in Methanol

A highly efficient method for the deacetylation of thioacetate is reported under mild acidic conditions employing acetyl chloride in methanol. Some of the major advantages are mild conditions, high efficiency, high yields, and easy operations.

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Bibliographic Details
Published inSynthetic communications Vol. 36; no. 13; pp. 1911 - 1914
Main Authors Tewari, Neera, Nizar, Hashim, Mane, Avinash, George, Vinod, Prasad, Mohan
Format Journal Article
LanguageEnglish
Published PHILADELPHIA Taylor & Francis Group 01.07.2006
Taylor & Francis
Subjects
Acetyl chloride
carbapenem intermediate
Chemistry
Chemistry, Organic
deacetylation
Physical Sciences
Science & Technology
thioacetate
thiol
MILD
thiol
deacetylation
acetyl chloride
carbapenem intermediate
LARGE-SCALE SYNTHESIS
thioacetate
CATALYTIC AMOUNT
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Summary:A highly efficient method for the deacetylation of thioacetate is reported under mild acidic conditions employing acetyl chloride in methanol. Some of the major advantages are mild conditions, high efficiency, high yields, and easy operations.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397910600602735