Hot pressing of bimodal alumina powders with magnesium aluminosilicate (MAS) addition

• Published in: Ceramics international Vol. 35; no. 4; pp. 1377 - 1383
• Main Authors: Li, Jiang, Pan, Yubai, Huang, Liping, Guo, Jingkun
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.05.2009
• Subjects: Bimodal alumina; Hot pressing; Mechanical properties; Microstructure; Mechanical properties; Hot pressing; Bimodal alumina; Microstructure
• ISSN: 0272-8842; 1873-3956
• DOI: 10.1016/j.ceramint.2008.07.002

High quality alumina ceramics were fabricated by hot-pressed sintering using bimodal alumina with superfine component as raw material and magnesium aluminosilicate (MAS) glass as sintering aid. Densification behavior, microstructure evolution and mechanical properties of alumina were investigated from 1300 °C to 1450 °C. The bimodal alumina powders were sintered to 99.8% of the theoretical value at 1400 °C and a comparative dense microstructure with a few plate-like abnormal grains was observed. With increase of sintering temperature up to 1450 °C, many fine matrix grains were consumed and quite a few abnormal grains impinged upon each other. For the alumina ceramics hot-pressed from bimodal alumina with 30 wt.% superfine component, optimal mechanical properties were obtained at 1400 °C. The bending strength and fracture toughness were 522 MPa and 5.0 MPa m 1/2, respectively.