Ti3SiC2-Cf composites by spark plasma sintering: Processing, microstructure and thermo-mechanical properties

• Published in: Journal of the European Ceramic Society Vol. 39; no. 9; pp. 2824 - 2830
• Main Authors: Lagos, M.A., Pellegrini, C., Agote, I., Azurmendi, N., Barcena, J., Parco, M., Silvestroni, L., Zoli, L., Sciti, D.
• Format: Journal Article
• Language: English
• Published: Elsevier Ltd 01.08.2019
• Subjects: Ceramic matrix composites; Interface; Max phases; Mechanical properties; Sintering; Spark plasma sintering; SPS; Ceramic matrix composites; Spark plasma sintering; Sintering; SPS; Mechanical properties; Max phases; Interface
• ISSN: 0955-2219; 1873-619X
• DOI: 10.1016/j.jeurceramsoc.2019.03.037

MAX phases, and particularly Ti3SiC2, are interesting for high temperature applications. The addition of carbon fibers can be used to reduce the density and to modify the properties of the matrix. This work presents the densification and characterization of Ti3SiC2 based composites with short carbon fibers using a fast and simple fabrication approach: dry mixing and densification by Spark Plasma Sintering. Good densification level was obtained below 1400 °C even with a high amount of fibers. The reaction of the fibers with the matrix is limited thanks to the fast processing time and depends on the amount of fibers in the composite. Bending strength at room temperature, between 437 and 120 MPa, is in the range of conventional CMCs with short fibers and according to the resistance of the matrix and the presence of residual porosity. Thermo-mechanical properties of the composites up to 1500 °C are also presented.