Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane

Reaction of the first homoleptic U(iii) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U(iii) to U(v) and isolation of a U(v) hydrazido complex. Corresponding U(v) imido, U(v) oxo, and U(iv) azido complexes were also synthesized for structural comparison.

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Published inChemical communications (Cambridge, England) Vol. 54; no. 77; pp. 10913 - 10916
Main Authors Settineri, Nicholas S, Shiau, Angela A, Arnold, John
Format Journal Article
LanguageEnglish
Published England Royal Society of Chemistry 2018
Royal Society of Chemistry (RSC)
Subjects
Crystallography
Oxidation
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Abstract Reaction of the first homoleptic U(iii) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U(iii) to U(v) and isolation of a U(v) hydrazido complex. Corresponding U(v) imido, U(v) oxo, and U(iv) azido complexes were also synthesized for structural comparison.
AbstractList Reaction of the first homoleptic U(iii) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U(iii) to U(v) and isolation of a U(v) hydrazido complex. Corresponding U(v) imido, U(v) oxo, and U(iv) azido complexes were also synthesized for structural comparison.
Use of a new homoleptic U( iii ) tris-guanidinate system stabilizes the formation of the first U( v ) hydrazido complex.
Reaction of the first homoleptic U( iii ) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U( iii ) to U( v ) and isolation of a U( v ) hydrazido complex. Corresponding U( v ) imido, U( v ) oxo, and U( iv ) azido complexes were also synthesized for structural comparison.
Author Shiau, Angela A
Settineri, Nicholas S
Arnold, John
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  contributor:
    fullname: Hayton
– volume: 6
  start-page: 6379
  year: 2015
  ident: C8CC06514D-(cit14)/*[position()=1]
  publication-title: Chem. Sci.
  doi: 10.1039/C5SC02150B
  contributor:
    fullname: Camp
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Snippet Reaction of the first homoleptic U(iii) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U(iii) to U(v) and isolation of a...
Reaction of the first homoleptic U( iii ) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U( iii ) to U( v ) and isolation...
Use of a new homoleptic U( iii ) tris-guanidinate system stabilizes the formation of the first U( v ) hydrazido complex.
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StartPage 10913
SubjectTerms Crystallography
Oxidation
Title Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane
URI https://www.ncbi.nlm.nih.gov/pubmed/30206592
https://www.proquest.com/docview/2111744746
https://search.proquest.com/docview/2102923858
https://www.osti.gov/biblio/1469716
Volume 54
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