Grain boundary faceting and abnormal grain growth in nickel

• Published in: Metallurgical and materials transactions. A, Physical metallurgy and materials science Vol. 31; no. 3; pp. 985 - 994
• Main Authors: SUNG BO LEE, NONG MOON HWANG, DUK YONG YOON, HENRY, M. F
• Format: Journal Article
• Language: English
• Published: New York, NY Springer 01.03.2000; Springer Nature B.V
• Subjects: Annealing; Applied sciences; Carburization (corrosion); Carburizing; Cold working, work hardening; annealing, post-deformation annealing, quenching, tempering recovery, and crystallization; Cold working, work hardening; annealing, quenching, tempering, recovery, and recrystallization; textures; Cross-disciplinary physics: materials science; rheology; Exact sciences and technology; Grain boundaries; Grain growth; Inclination angle; Materials science; Melting points; Metals. Metallurgy; Physics; Recrystallization; Treatment of materials and its effects on microstructure and properties; Grain boundaries; Grain growth; Transition elements; Recrystallization; Polycrystals; Nickel; Experimental study; Microstructure; Thermal annealing; Faceting
• ISSN: 1073-5623; 1543-1940
• DOI: 10.1007/s11661-000-0040-3

A correlation between grain boundary faceting and abnormal grain growth has been observed in recrystallized polycrystalline Ni at varying annealing temperatures, with or without C added. Carburized Ni specimens deformed to 50 pct show faceted grain boundaries and abnormal grain growth when annealed at temperatures below 0.7 Tm, where Tm is the melting point of Ni in absolute scale. When annealed at or above 0.7 Tm, the grain boundaries are smoothly curved and, therefore, have a rough structure, and normal grain growth is observed. In the specimens annealed in vacuum without carburization, all grain boundaries are faceted at 0.55 Tm, and some of them become defaceted at higher temperatures. The specimens annealed in vacuum at temperatures between 0.55 and 0.95 Tm show abnormal grain growth. When the grain boundaries have a rough structure and are, therefore, nearly isotropic, normal grain growth is indeed expected, as shown by the simulation and analytical treatment. When all or a fraction of the grain boundaries are faceted, with the facet planes corresponding to the singular cusp directions in the variation of the boundary energy against the inclination angle, abnormal grain growth can occur either because some grain boundary junctions become immobile due to a torque effect, or the growth occurs by a step mechanism.