Visible-light-induced decarboxylative acylation of quinoxalin-2(1)-ones with α-oxo carboxylic acids under metal-, strong oxidant- and external photocatalyst-free conditions
A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1 H )-ones and α-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosen...
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| Published in | Green chemistry : an international journal and green chemistry resource : GC Vol. 22; no. 5; pp. 172 - 1725 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
CAMBRIDGE
Royal Soc Chemistry
09.03.2020
Royal Society of Chemistry |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1
H
)-ones and α-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosensitizers, ultimately reducing the generation of waste.
An eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1
H
)-ones and α-oxo carboxylic acids with air as the oxidant under external-photocatalyst-free conditions was established. |
|---|---|
| AbstractList | A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1H)-ones and α-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosensitizers, ultimately reducing the generation of waste. A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1 H )-ones and α-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosensitizers, ultimately reducing the generation of waste. An eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1 H )-ones and α-oxo carboxylic acids with air as the oxidant under external-photocatalyst-free conditions was established. A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1 H )-ones and α-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosensitizers, ultimately reducing the generation of waste. A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1H)-ones and alpha-oxo carboxylic acids with ambient air as the sole oxidant at room temperature was established. The reaction proceeded efficiently without any metal catalysts, strong oxidants or external-photosensitizers, ultimately reducing the generation of waste. |
| Author | Bai, You-Shu He, Wei-Min Tang, Hai-Shan Xu, Xiang-Qin Peng, Xia Lin, Ying-Wu Huang, Ying Xie, Long-Yong Cao, Zhong |
| AuthorAffiliation | Department of Chemistry Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation University of South China Changsha University of Science and Technology Hunan University of Science and Engineering School of Chemistry and Chemical Engineering |
| AuthorAffiliation_xml | – name: Changsha University of Science and Technology – name: Hunan University of Science and Engineering – name: Department of Chemistry – name: School of Chemistry and Chemical Engineering – name: University of South China – name: Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation |
| Author_xml | – sequence: 1 givenname: Long-Yong surname: Xie fullname: Xie, Long-Yong – sequence: 2 givenname: You-Shu surname: Bai fullname: Bai, You-Shu – sequence: 3 givenname: Xiang-Qin surname: Xu fullname: Xu, Xiang-Qin – sequence: 4 givenname: Xia surname: Peng fullname: Peng, Xia – sequence: 5 givenname: Hai-Shan surname: Tang fullname: Tang, Hai-Shan – sequence: 6 givenname: Ying surname: Huang fullname: Huang, Ying – sequence: 7 givenname: Ying-Wu surname: Lin fullname: Lin, Ying-Wu – sequence: 8 givenname: Zhong surname: Cao fullname: Cao, Zhong – sequence: 9 givenname: Wei-Min surname: He fullname: He, Wei-Min |
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| Keywords | ALCOHOLS THIOLS AMINATION QUINOXALIN-2(H)-ONES QUINOXALINONES PHOSPHONATION ARYLATION 3-ARYLATION C-H TRIFLUOROMETHYLATION CYCLIZATION |
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| Snippet | A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1
H
)-ones and α-oxo carboxylic acids with ambient air as the sole... A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1H)-ones and alpha-oxo carboxylic acids with ambient air as the sole... A mild and eco-friendly visible-light-induced decarboxylative acylation of quinoxalin-2(1H)-ones and α-oxo carboxylic acids with ambient air as the sole... |
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| SubjectTerms | Acylation air Air temperature ambient temperature Carboxylic acids Catalysts Chemistry Chemistry, Multidisciplinary Green & Sustainable Science & Technology Green chemistry Light effects Oxidants Oxidizing agents Physical Sciences Room temperature Science & Technology Science & Technology - Other Topics wastes |
| Title | Visible-light-induced decarboxylative acylation of quinoxalin-2(1)-ones with α-oxo carboxylic acids under metal-, strong oxidant- and external photocatalyst-free conditions |
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