Microwave assisted synthesis of 10b-aza-10c-borapyrene

The synthesis of 10b-aza-10c-borapyrene, an analog of the polycyclic aromatic hydrocarbon pyrene with an internal boron–nitrogen bond, has been improved. We have dramatically reduced the reaction times and ease of workup for the synthesis of this molecule by using a microwave reactor and carefully c...

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Bibliographic Details
Published inTetrahedron letters Vol. 55; no. 2; pp. 445 - 447
Main Authors Wadle, Jonathan J., McDermott, Logan B., Fort, Eric H.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 08.01.2014
Subjects
Azaborine
Bonding
Microwave-assisted synthesis
Microwaves
Polycyclic aromatic hydrocarbon analogs
Polycyclic aromatic hydrocarbons
Pyrene
Pyrenes
Reaction time
Reactors
Synthesis (chemistry)
Tetrahedrons
PYHBJABFWFUDGW-UHFFFAOYSA-N
Pyrene
GMPHJDOWRALMEC-UHFFFAOYSA-N
VYRLFYTZNXGQIK-UHFFFAOYSA-N
Microwave-assisted synthesis
FOYPKVVSTKSTGR-UHFFFAOYSA-N
Polycyclic aromatic hydrocarbon analogs
Azaborine
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Summary:The synthesis of 10b-aza-10c-borapyrene, an analog of the polycyclic aromatic hydrocarbon pyrene with an internal boron–nitrogen bond, has been improved. We have dramatically reduced the reaction times and ease of workup for the synthesis of this molecule by using a microwave reactor and carefully controlling reaction conditions.
Bibliography:ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2013.11.052