Efficient synthesis of N,N’-methylenebisglycolurils

Coupling of 6-(carboxy)alkyl-2,4-dialkylglycolurils with N-(hydroxymethyl)glycolurils gives N,N’-methylenebisglycolurils totally substituted at the nitrogen atoms, which are formed mostly as racemate diastereomers.

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Bibliographic Details
Published inMendeleev communications Vol. 26; no. 2; pp. 136 - 138
Main Authors Kravchenko, Angelina N., Chikunov, Ilya E., Gazieva, Galina A., Makhova, Nina N.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.03.2016
Subjects
Coupling
Nitrogen atoms
Synthesis
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Summary:Coupling of 6-(carboxy)alkyl-2,4-dialkylglycolurils with N-(hydroxymethyl)glycolurils gives N,N’-methylenebisglycolurils totally substituted at the nitrogen atoms, which are formed mostly as racemate diastereomers.
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ISSN:0959-9436
DOI:10.1016/j.mencom.2016.03.018