Nonaqueous preparation of nanocomposite films containing both polyoxometalate and phthalocyanine with bifunctional electrocatalytic properties

New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P 2W 18) were successfully fabricated using the electrostatic layer-by-layer (LbL) assembled method in nonaqueous (DMF) media. UV–vis spectroscopy, IR spectrosc...

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Published inMaterials letters Vol. 63; no. 6; pp. 608 - 610
Main Authors Yang, Yaobin, Xu, Lin, Xu, Bingbing, Du, Xiguang, Guo, Weihua
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.03.2009
Subjects
Bifunctional electrocatalytic
Layer-by-layer
Multilayer structure
Nanocomposites
Nonaqueous
Polyoxometalate
Polyoxometalate
Bifunctional electrocatalytic
Nanocomposites
Multilayer structure
Nonaqueous
Layer-by-layer
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Abstract New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P 2W 18) were successfully fabricated using the electrostatic layer-by-layer (LbL) assembled method in nonaqueous (DMF) media. UV–vis spectroscopy, IR spectroscopy, X-ray photoelectron spectroscopy, atomic force microscopy (AFM) and electrochemical method were used to characterize the assembled multilayer films. UV–vis measurements revealed regular film growth with each four-layer {P 2W 18/CoTAPc/PSS/PAH} adsorption. AFM analysis provides the morphology of the multilayer films. The cyclic voltammetric curves indicate that the film shows electrocatalytic activity for chlorate anion.
AbstractList New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P2W18) were successfully fabricated using the electrostatic layer-by-layer (LbL) assembled method in nonaqueous (DMF) media. UV-vis spectroscopy, IR spectroscopy, X-ray photoelectron spectroscopy, atomic force microscopy (AFM) and electrochemical method were used to characterize the assembled multilayer films. UV-vis measurements revealed regular film growth with each four-layer {P2W18/CoTAPc/PSS/PAH} adsorption. AFM analysis provides the morphology of the multilayer films. The cyclic voltammetric curves indicate that the film shows electrocatalytic activity for chlorate anion.
New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P 2W 18) were successfully fabricated using the electrostatic layer-by-layer (LbL) assembled method in nonaqueous (DMF) media. UV–vis spectroscopy, IR spectroscopy, X-ray photoelectron spectroscopy, atomic force microscopy (AFM) and electrochemical method were used to characterize the assembled multilayer films. UV–vis measurements revealed regular film growth with each four-layer {P 2W 18/CoTAPc/PSS/PAH} adsorption. AFM analysis provides the morphology of the multilayer films. The cyclic voltammetric curves indicate that the film shows electrocatalytic activity for chlorate anion.
Author Du, Xiguang
Yang, Yaobin
Guo, Weihua
Xu, Lin
Xu, Bingbing
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Nanocomposites
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Snippet New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P 2W 18) were...
New bifunctional nanocomposite films containing water-insolvable cobalt tetraaminophthalocyanine (CoTAPc) and 2:18 tungstophosphate anions (P2W18) were...
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SubjectTerms Bifunctional electrocatalytic
Layer-by-layer
Multilayer structure
Nanocomposites
Nonaqueous
Polyoxometalate
Title Nonaqueous preparation of nanocomposite films containing both polyoxometalate and phthalocyanine with bifunctional electrocatalytic properties
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