Evolution of the microstructure and fracture characteristics of a Mg-Nd-Zn-Zr-Mn alloy through heat treatment and extrusion

• Published in: Journal of alloys and compounds Vol. 765; pp. 470 - 479
• Main Authors: Gui, Zhenzhen, Kang, Zhixin, Li, Yuanyuan
• Format: Journal Article
• Language: English
• Published: Lausanne Elsevier B.V 15.10.2018; Elsevier BV
• Subjects: Alloy systems; Biodegradability; Ductile fracture; Elongation; Evolution; Extrusion; Fracture characteristics; Fracture pathway; Fractures; Grain boundaries; Heat treating; Heat treatment; Hot extrusion; Intergranular fracture; Magnesium base alloys; Manganese base alloys; Mechanical properties; Mechanical property; Mg-Nd-Zn-Zr-Mn; Microstructure; Multiscale microstructure; Precipitates; Precipitation hardening; Pressure casting; SEM/TEM; Solid solutions; Solution strengthening; Tensile properties; Zinc; Zirconium; Fracture characteristics; Multiscale microstructure; Fracture pathway; Mg-Nd-Zn-Zr-Mn; Mechanical property; SEM/TEM
• ISSN: 0925-8388; 1873-4669
• DOI: 10.1016/j.jallcom.2018.06.185

Appropriate mechanical properties are essential for the use of biodegradable Mg-based alloys as structurally supporting materials. However, research studies on the evolution of the tensile fracture pathways and fracture characteristics of as-cast and as-extruded Mg-based alloys are limited. In this paper, the microstructures, tensile properties, fracture pathways and fracture characteristics of the as-cast, heat treated and hot-extruded Mg-1.59Nd-2.91Zn-0.05Zr-0.35Mn (NZKM) alloys were systematically investigated. The results indicated that the hot-extruded NZKM alloy exhibits good mechanical properties with a yield strength and an elongation reaching 212 MPa and 30.7%, respectively. These excellent properties were attributed to its special multiscale microstructure consisting of an α-Mg matrix (2–10 μm), eutectic compound β-Mg4Zn7 (2–10 μm) together with a high density of dispersed nanoscale precipitates, that provide solid solution strengthening, grain boundary strengthening and precipitation strengthening effects. The fracture patterns changed with the evolution of the microstructures. Intergranular and transgranular cleavage fractures were changed to ductile fractures by hot extrusion. [Display omitted] •Hot extrusion enhanced mechanical properties of Mg-Nd-Zn-Zr-Mn (NZKM) alloy.•Great mechanical properties because of dislocations and deformation twins.•Morphologies of eutectic compounds and grain sizes affect fracture behaviors.