Preparation of nano α-alumina powder and wear resistance of nanoparticles reinforced composite coating

• Published in: Powder technology Vol. 257; pp. 83 - 87
• Main Authors: Chen, Caifeng, Ding, Zhidan, Tan, Qi, Qi, Henghua, He, Yonghui
• Format: Journal Article
• Language: English
• Published: Amsterdam Elsevier B.V 01.05.2014; Elsevier
• Subjects: Applied sciences; Chemical engineering; Coating; Exact sciences and technology; Miscellaneous; Nano; Preparation; Solid-solid systems; Thermal spraying; α-Alumina; Nano; Thermal spraying; α-Alumina; Coating; Preparation; Volume fraction; Nanoparticle; Spraying; Long term; Precursor; Dispersion; Composite material; Powder; Calcining; Abrasive wear; Activated carbon; Morphology; Wear resistance
• ISSN: 0032-5910; 1873-328X
• DOI: 10.1016/j.powtec.2014.02.059

Nanometer α-alumina powder was synthesized using the pore rich activated carbon as the reaction place, and the α-alumina nanoparticle reinforced nickel based composite coating was prepared by flash thermal spray method. The composite coating was abraded on abrasive wear-machine to study its wear resistance property. The results showed that a large number of uniform size spherical-shaped precursor particles were in the activated carbon pores, which could be long-term stable in a spherical shape and adsorbed on the pore wall. In addition, activated carbon pores could prevent the alumina particles from growing up and reuniting effectively during the precursor particles calcination process. And the activated carbon had completely burned at high temperature as well. Finally, nano α-alumina powder with good dispersion was obtained. The wear resistance of the nickel based composite coating was reinforced by the nanometer α-alumina powder. With 2% volume fraction addition of nanometer α-alumina, the coating has the best abrasive wear resistance property. A large number of alumina precursor particles were synthesized in the pores of the activated carbon template, which could be long-term stable in a spherical shape. The template had completely burned at high temperature, and nano α-alumina powder with good dispersion was obtained. The wear resistance of the nickel based coating was reinforced by the powder. [Display omitted] •The activated carbon has rich pores after activated by zinc chloride.•Mono-dispersed precursor particles can exist stably in the pores.•The pores prevent the particles from growing up and reuniting.•The nanometer α-Al2O3powder with good dispersion was obtained.•The wear resistance of the coating was reinforced by the nanometer-α-alumina powder.