Visible-light-initiated malic acid-promoted cascade coupling/cyclization of aromatic amines and KSCN to 2-aminobenzothiazoles without photocatalyst

A simple and practical method for the synthesis of 2-aminobenzothiazoles through visible-light-initiated malic acid-promoted cascade coupling/cyclization of aromatic amines and KSCN with ambient air as an oxidant in eco-friendly bis(methoxypropy) ether at ambient temperature was developed. [Display...

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Published inChinese chemical letters Vol. 31; no. 7; pp. 1895 - 1898
Main Authors He, Wei-Bao, Gao, Lan-Qing, Chen, Xin-Jie, Wu, Zhi-Lin, Huang, Ying, Cao, Zhong, Xu, Xin-Hua, He, Wei-Min
Format Journal Article
LanguageEnglish
Published NEW YORK Elsevier B.V 01.07.2020
Elsevier
Department of Chemistry, Hunan University, Changsha 410082, China%School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China%School of Chemistry and Chemical Engineering,University of South China%Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology,Changsha 410114, China
Subjects
2-Aminobenzothiazoles
Air
Cascade reaction
Chemistry
Chemistry, Multidisciplinary
Photocatalysis
Photocatalyst-free
Physical Sciences
Science & Technology
Cascade reaction
2-Aminobenzothiazoles
Photocatalyst-free
Air
Photocatalysis
OXIDATION
DESIGN
CATALYST-FREE
HYDROXYLATION
EFFICIENT SYNTHESIS
REDUCTIVE MINISCI REACTION
METAL
QUINOXALIN-2(1H)-ONES
DERIVATIVES
MOLECULAR-OXYGEN
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Abstract A simple and practical method for the synthesis of 2-aminobenzothiazoles through visible-light-initiated malic acid-promoted cascade coupling/cyclization of aromatic amines and KSCN with ambient air as an oxidant in eco-friendly bis(methoxypropy) ether at ambient temperature was developed. [Display omitted] By using ambient air as the oxidant and malic acid as the promoter, a practical method for the preparation of 2-aminobenzothiazoles through visible-light-initiated cascade reaction of aromatic amines and KSCN in eco-friendly bis(methoxypropy)ether under metal-, hazardous additive-, photocatalyst-free conditions was established.
AbstractList By using ambient air as the oxidant and malic acid as the promoter, a practical method for the preparation of 2-aminobenzothiazoles through visible-light-initiated cascade reaction of aromatic amines and KSCN in eco-friendly bis(methoxypropy)ether under metal-, hazardous additive-, photocatalyst-free conditions was established. (C) 2020 Chinese Chemical Society and Institute of Materia Medica, Chinese Academy of Medical Sciences. Published by Elsevier B.V. All rights reserved.
By using ambient air as the oxidant and malic acid as the promoter,a practical method for the preparation of 2-aminobenzothiazoles through visible-light-initiated cascade reaction of aromatic amines and KSCN in eco-friendly bis(methoxypropy)ether under metal-,hazardous additive-,photocatalyst-free conditions was established.
A simple and practical method for the synthesis of 2-aminobenzothiazoles through visible-light-initiated malic acid-promoted cascade coupling/cyclization of aromatic amines and KSCN with ambient air as an oxidant in eco-friendly bis(methoxypropy) ether at ambient temperature was developed. [Display omitted] By using ambient air as the oxidant and malic acid as the promoter, a practical method for the preparation of 2-aminobenzothiazoles through visible-light-initiated cascade reaction of aromatic amines and KSCN in eco-friendly bis(methoxypropy)ether under metal-, hazardous additive-, photocatalyst-free conditions was established.
Author He, Wei-Bao
Wu, Zhi-Lin
Gao, Lan-Qing
He, Wei-Min
Chen, Xin-Jie
Xu, Xin-Hua
Huang, Ying
Cao, Zhong
AuthorAffiliation Department of Chemistry, Hunan University, Changsha 410082, China%School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China%School of Chemistry and Chemical Engineering,University of South China%Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology,Changsha 410114, China
AuthorAffiliation_xml – name: Department of Chemistry, Hunan University, Changsha 410082, China%School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China%School of Chemistry and Chemical Engineering,University of South China%Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology,Changsha 410114, China
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  organization: Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology, Changsha 410114, China
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Issue 7
Keywords Cascade reaction
2-Aminobenzothiazoles
Photocatalyst-free
Air
Photocatalysis
OXIDATION
DESIGN
CATALYST-FREE
HYDROXYLATION
EFFICIENT SYNTHESIS
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METAL
QUINOXALIN-2(1H)-ONES
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Department of Chemistry, Hunan University, Changsha 410082, China%School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China%School of Chemistry and Chemical Engineering,University of South China%Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology,Changsha 410114, China
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– name: Department of Chemistry, Hunan University, Changsha 410082, China%School of Chemistry and Chemical Engineering, Hunan University of Science and Technology, Xiangtan 411201, China%School of Chemistry and Chemical Engineering,University of South China%Hunan Provincial Key Laboratory of Materials Protection for Electric Power and Transportation, Changsha University of Science and Technology,Changsha 410114, China
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Snippet A simple and practical method for the synthesis of 2-aminobenzothiazoles through visible-light-initiated malic acid-promoted cascade coupling/cyclization of...
By using ambient air as the oxidant and malic acid as the promoter, a practical method for the preparation of 2-aminobenzothiazoles through...
By using ambient air as the oxidant and malic acid as the promoter,a practical method for the preparation of 2-aminobenzothiazoles through...
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SubjectTerms 2-Aminobenzothiazoles
Air
Cascade reaction
Chemistry
Chemistry, Multidisciplinary
Photocatalysis
Photocatalyst-free
Physical Sciences
Science & Technology
Title Visible-light-initiated malic acid-promoted cascade coupling/cyclization of aromatic amines and KSCN to 2-aminobenzothiazoles without photocatalyst
URI https://dx.doi.org/10.1016/j.cclet.2020.02.011
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