Synthesis of heteroatom and metallic compound self-co-doped porous carbon derived from swine manure for supercapacitor electrodes and lead ion adsorbents

[Display omitted] •SMACs with different structures and heteroatom contents were obtained.•SMACHF with a SSA of 2321 m2/g exhibited the highest specific capacitance of 278 F/g.•Excellent Pb2+ adsorption of 211.8 mg/g by SMACNON was obtained.•Heteroatoms and metallic elements improved the capacitance...

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Published inJournal of industrial and engineering chemistry (Seoul, Korea) Vol. 102; pp. 195 - 205
Main Authors Qin, Liyuan, Wu, Yang, Hou, Zhiwei, Zhang, Shihui, Jiang, Enchen
Format Journal Article
LanguageEnglish
Published Elsevier B.V 25.10.2021
한국공업화학회
Subjects
Electrochemical performance
Metallic elements and heteroatoms
Pb2+ adsorption
Porous carbon
Self-co-doped
Swine manure
화학공학
Electrochemical performance
Pb2+ adsorption
Porous carbon
Self-co-doped
Metallic elements and heteroatoms
Swine manure
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Abstract [Display omitted] •SMACs with different structures and heteroatom contents were obtained.•SMACHF with a SSA of 2321 m2/g exhibited the highest specific capacitance of 278 F/g.•Excellent Pb2+ adsorption of 211.8 mg/g by SMACNON was obtained.•Heteroatoms and metallic elements improved the capacitance retention by 100% after 10,000 cycles. Swine manure activated carbon (SMAC) with self-co-doped metallic compounds and heteroatoms was prepared by combining KOH activation with pyrolysis. The structure, electrochemical performance and adsorption of SMACs prepared with various activation temperatures, activation times, alkali-carbon ratios and pickling steps were investigated. A hierarchical pore structure existed in all the SMACs, which showed excellent and significantly different properties, including a specific capacitance of 278 F/g, and a high SSA of 2321 m2/g (SMACHF), which retained 100% of its capacitance after 10,000 cycles at 5 A/g and a Pb2+ adsorption capacity of 211.8 mg/g at room temperature (SMACNON). The SMACs contained heteroatom functional groups and Si, Ca and Mg compounds, which did not produce pseudocapacitors but did increase the Pb2+ adsorption capacity and electrochemical cycling stability. The Pb2+ adsorption capacities of SMACNON, SMACPHF and SMACHF corresponded to the effect of the functional group content rather than the effect of the SSA. These porous carbons were derived from inexpensive swine manure, combine suitable porosity with metallic elements and heteroatom doping, and have promising uses in multifunctional applications.
AbstractList [Display omitted] •SMACs with different structures and heteroatom contents were obtained.•SMACHF with a SSA of 2321 m2/g exhibited the highest specific capacitance of 278 F/g.•Excellent Pb2+ adsorption of 211.8 mg/g by SMACNON was obtained.•Heteroatoms and metallic elements improved the capacitance retention by 100% after 10,000 cycles. Swine manure activated carbon (SMAC) with self-co-doped metallic compounds and heteroatoms was prepared by combining KOH activation with pyrolysis. The structure, electrochemical performance and adsorption of SMACs prepared with various activation temperatures, activation times, alkali-carbon ratios and pickling steps were investigated. A hierarchical pore structure existed in all the SMACs, which showed excellent and significantly different properties, including a specific capacitance of 278 F/g, and a high SSA of 2321 m2/g (SMACHF), which retained 100% of its capacitance after 10,000 cycles at 5 A/g and a Pb2+ adsorption capacity of 211.8 mg/g at room temperature (SMACNON). The SMACs contained heteroatom functional groups and Si, Ca and Mg compounds, which did not produce pseudocapacitors but did increase the Pb2+ adsorption capacity and electrochemical cycling stability. The Pb2+ adsorption capacities of SMACNON, SMACPHF and SMACHF corresponded to the effect of the functional group content rather than the effect of the SSA. These porous carbons were derived from inexpensive swine manure, combine suitable porosity with metallic elements and heteroatom doping, and have promising uses in multifunctional applications.
Swine manure activated carbon (SMAC) with self-co-doped metallic compounds and heteroatoms wasprepared by combining KOH activation with pyrolysis. The structure, electrochemical performance andadsorption of SMACs prepared with various activation temperatures, activation times, alkali-carbonratios and pickling steps were investigated. A hierarchical pore structure existed in all the SMACs, whichshowed excellent and significantly different properties, including a specific capacitance of 278 F/g, and ahigh SSA of 2321 m2/g (SMACHF), which retained 100% of its capacitance after 10,000 cycles at 5 A/g and aPb2+ adsorption capacity of 211.8 mg/g at room temperature (SMACNON). The SMACs contained heteroatomfunctional groups and Si, Ca and Mg compounds, which did not produce pseudocapacitors but didincrease the Pb2+ adsorption capacity and electrochemical cycling stability. The Pb2+ adsorption capacitiesof SMACNON, SMACPHF and SMACHF corresponded to the effect of the functional group content ratherthan the effect of the SSA. These porous carbons were derived from inexpensive swine manure, combinesuitable porosity with metallic elements and heteroatom doping, and have promising uses in multifunctionalapplications. KCI Citation Count: 1
Author Hou, Zhiwei
Wu, Yang
Zhang, Shihui
Jiang, Enchen
Qin, Liyuan
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  givenname: Enchen
  surname: Jiang
  fullname: Jiang, Enchen
  email: enchenjiang@hotmail.com
  organization: College of Engineering, Northeast Agricultural University, Harbin 150030, China
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Keywords Electrochemical performance
Pb2+ adsorption
Porous carbon
Self-co-doped
Metallic elements and heteroatoms
Swine manure
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Snippet [Display omitted] •SMACs with different structures and heteroatom contents were obtained.•SMACHF with a SSA of 2321 m2/g exhibited the highest specific...
Swine manure activated carbon (SMAC) with self-co-doped metallic compounds and heteroatoms wasprepared by combining KOH activation with pyrolysis. The...
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SubjectTerms Electrochemical performance
Metallic elements and heteroatoms
Pb2+ adsorption
Porous carbon
Self-co-doped
Swine manure
화학공학
Title Synthesis of heteroatom and metallic compound self-co-doped porous carbon derived from swine manure for supercapacitor electrodes and lead ion adsorbents
URI https://dx.doi.org/10.1016/j.jiec.2021.06.038
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