Synthesis and Molecular Structure of 2-(4-Chlorophenyl)-3-(phenyl-amino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one
2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4 H -imidazol-4-one, C 20 H 14 N 3 OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P 1, Z = 2. All three rings are planar, and imidazole...
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| Published in | Crystallography reports Vol. 62; no. 7; pp. 1148 - 1151 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
01.12.2017
Springer Nature B.V |
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| Abstract | 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4
H
-imidazol-4-one, C
20
H
14
N
3
OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr.
P
1, Z = 2. All three rings are planar, and imidazole ring is almost perpendicular to the phenyl ring with the dihedral angle of 88.65(2)°. In the crystal, pairs of O–H···O hydrogen bonds link molecules into inversion dimers, featuring R
22
(10) graph set motif. Crystal structure is further stabilized by π···π interactions. |
|---|---|
| AbstractList | 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C20H14N3OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P1, Z = 2. All three rings are planar, and imidazole ring is almost perpendicular to the phenyl ring with the dihedral angle of 88.65(2)°. In the crystal, pairs of O–H···O hydrogen bonds link molecules into inversion dimers, featuring R22(10) graph set motif. Crystal structure is further stabilized by π···π interactions. 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4 H -imidazol-4-one, C 20 H 14 N 3 OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P 1, Z = 2. All three rings are planar, and imidazole ring is almost perpendicular to the phenyl ring with the dihedral angle of 88.65(2)°. In the crystal, pairs of O–H···O hydrogen bonds link molecules into inversion dimers, featuring R 22 (10) graph set motif. Crystal structure is further stabilized by π···π interactions. 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C{sub 20}H{sub 14}N{sub 3}OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P1, Z = 2. All three rings are planar, and imidazole ring is almost perpendicular to the phenyl ring with the dihedral angle of 88.65(2)°. In the crystal, pairs of O–H···O hydrogen bonds link molecules into inversion dimers, featuring R{sub 22}(10) graph set motif. Crystal structure is further stabilized by π···π interactions. |
| Author | Narayana, B. Anthal, Sumati Sarojini, B. K. Kant, R. Sharma, Devinder K. Subbulakshmi, K. N. |
| Author_xml | – sequence: 1 givenname: Devinder K. surname: Sharma fullname: Sharma, Devinder K. organization: Department of Physics, University, X-ray Crystallography Laboratory – sequence: 2 givenname: K. N. surname: Subbulakshmi fullname: Subbulakshmi, K. N. organization: Department of Chemistry, Mangalore University – sequence: 3 givenname: B. surname: Narayana fullname: Narayana, B. organization: Department of Chemistry, Mangalore University – sequence: 4 givenname: B. K. surname: Sarojini fullname: Sarojini, B. K. organization: Department of Industrial Chemistry, Mangalore University – sequence: 5 givenname: Sumati surname: Anthal fullname: Anthal, Sumati organization: Department of Physics, University, X-ray Crystallography Laboratory – sequence: 6 givenname: R. surname: Kant fullname: Kant, R. email: rkant.ju@gmail.com organization: Department of Physics, University, X-ray Crystallography Laboratory |
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| Snippet | 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4
H
-imidazol-4-one, C
20
H
14
N
3
OSCl was synthesized and its crystal structure... 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C20H14N3OSCl was synthesized and its crystal structure was... 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C{sub 20}H{sub 14}N{sub 3}OSCl was synthesized and its crystal... |
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| SubjectTerms | Chemical bonds Chemical synthesis CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY CRYSTAL STRUCTURE Crystallography and Scattering Methods Dihedral angle DIMERS HYDROGEN Hydrogen bonds Imidazole IMIDAZOLES INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY MOLECULAR STRUCTURE MOLECULES MONOCRYSTALS Physics Physics and Astronomy RINGS Single crystals Structure of Organic Compounds SYNTHESIS X-RAY DIFFRACTION |
| Title | Synthesis and Molecular Structure of 2-(4-Chlorophenyl)-3-(phenyl-amino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one |
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