Protection-deprotection method in synthesis of calixarene derivatives

The debenzylation and selective de-tert-butylation of p-tert-calix[4]arene derivatives were studied and 11,17,23-tri-tert-butyl-25,26,27-tri-O-etherated calix[4]arenes were synthesized by a simultaneous debenzylation and selective de-tert-butylation process.

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Bibliographic Details
Published inChinese journal of chemistry Vol. 18; no. 2; pp. 207 - 211
Main Authors Lu, GY, Li, Q, Liu, F, Wan, XB
Format Journal Article
LanguageEnglish
Published BEIJING Science Press 01.03.2000
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Summary:The debenzylation and selective de-tert-butylation of p-tert-calix[4]arene derivatives were studied and 11,17,23-tri-tert-butyl-25,26,27-tri-O-etherated calix[4]arenes were synthesized by a simultaneous debenzylation and selective de-tert-butylation process.
ISSN:1001-604X
DOI:10.1002/cjoc.20000180214