Thermal and structural analysis of 4,5,6-trimethoxyisatin

4,5,6-Trimethoxyisatin was crystallized from water to give dark red needles that were characterized by NMR and IR spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), single-crystal X-ray diffraction (XRD) and hot-stage microscopy.

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Bibliographic Details
Published inJournal of molecular structure Vol. 932; no. 1; pp. 38 - 42
Main Authors Oliveira-Campos, Ana M.F., Rodrigues, Lígia M., Francisco, Carla S., Oliveira, Maria Jovita, Silva, M. Manuela, Smith, Michael J., Paz, Filipe A. Almeida
Format Journal Article
LanguageEnglish
Published Elsevier B.V 27.08.2009
Subjects
DSC
Hot-stage microscopy
Isatin
Single-crystal X-ray diffraction (XRD)
TGA
Hot-stage microscopy
Single-crystal X-ray diffraction (XRD)
DSC
Isatin
TGA
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Summary:4,5,6-Trimethoxyisatin was crystallized from water to give dark red needles that were characterized by NMR and IR spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), single-crystal X-ray diffraction (XRD) and hot-stage microscopy.
ISSN:0022-2860
1872-8014
DOI:10.1016/j.molstruc.2009.05.038