Modern solid state NMR techniques and concepts in structural studies of synthetic polymers

In this mini‐review, we present the solid state nuclear magnetic resonance (NMR) methods which trace the new tendency in structural studies of synthetic polymers. The review is organized into three sections. In the first part, short theoretical background and introduction to very fast magic angle sp...

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Bibliographic Details
Published inPolymers for advanced technologies Vol. 27; no. 9; pp. 1143 - 1155
Main Authors Kaźmierski, S., Pawlak, T., Jeziorna, A., Potrzebowski, M. J.
Format Journal Article
LanguageEnglish
Published Bognor Regis Blackwell Publishing Ltd 01.09.2016
Wiley Subscription Services, Inc
Subjects
Atomic structure
Crystallography
dynamic nuclear polarization
Dynamics
NMR crystallography
Nuclear magnetic resonance
Polarization
Polymers
Solid state
solid state NMR
Spinning
synthetic polymers
very fast MAS
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Summary:In this mini‐review, we present the solid state nuclear magnetic resonance (NMR) methods which trace the new tendency in structural studies of synthetic polymers. The review is organized into three sections. In the first part, short theoretical background and introduction to very fast magic angle spinning NMR technique with sample rotation 60 kHz are shown. The second part presents method for enhancing the sensitivity of NMR experiments by application of dynamic nuclear polarization magic angle spinning technique. In the third section, the power of the NMR crystallography approach which can be used for fine refinement of polymers structure on the atomic level is discussed. Copyright © 2016 John Wiley & Sons, Ltd.
Bibliography:istex:E391E1510390C95A94CFCACCBD79655F6C96AE0C
ark:/67375/WNG-M19B6HBM-L
ArticleID:PAT3780
ObjectType-Article-1
SourceType-Scholarly Journals-1
ObjectType-Feature-2
content type line 23
ISSN:1042-7147
1099-1581
DOI:10.1002/pat.3780