Grafting stimuli-responsive polymer brushes to freshly-etched porous silicon

This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of freshly‐etched porous Si. Grafting is achieved by pre‐hydrosilylation of the hydride‐terminated porous Si with undecylenic acid. The end carboxyl groups ar...

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Published inPhysica status solidi. C Vol. 6; no. 7; pp. 1717 - 1720
Main Authors Segal, Ester, Perelman, Loren A., Moore, Troy, Kesselman, Ellina, Sailor, Michael J.
Format Journal Article
LanguageEnglish
Published Berlin WILEY-VCH Verlag 01.07.2009
WILEY‐VCH Verlag
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81.05.Rm
81.07.Pr
82.35.Gh
82.35.Pq
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Abstract This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of freshly‐etched porous Si. Grafting is achieved by pre‐hydrosilylation of the hydride‐terminated porous Si with undecylenic acid. The end carboxyl groups are activated and reacted with amine‐terminated poly(N‐isopropylacrylamide). Attachment of the polymer to the porous Si is confirmed by Fourier‐transform infrared (FTIR) spectroscopy and atomic force microscopy. (© 2009 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
AbstractList This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of freshly‐etched porous Si. Grafting is achieved by pre‐hydrosilylation of the hydride‐terminated porous Si with undecylenic acid. The end carboxyl groups are activated and reacted with amine‐terminated poly(N‐isopropylacrylamide). Attachment of the polymer to the porous Si is confirmed by Fourier‐transform infrared (FTIR) spectroscopy and atomic force microscopy. (© 2009 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
Abstract This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of freshly‐etched porous Si. Grafting is achieved by pre‐hydrosilylation of the hydride‐terminated porous Si with undecylenic acid. The end carboxyl groups are activated and reacted with amine‐terminated poly(N‐isopropylacrylamide). Attachment of the polymer to the porous Si is confirmed by Fourier‐transform infrared (FTIR) spectroscopy and atomic force microscopy. (© 2009 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)
Author Sailor, Michael J.
Segal, Ester
Perelman, Loren A.
Kesselman, Ellina
Moore, Troy
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crossref_primary_10_1021_acs_biomac_0c01318
crossref_primary_10_1016_j_mseb_2013_05_001
crossref_primary_10_1021_acs_langmuir_5b03794
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Snippet This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of freshly‐etched...
Abstract This work describes a simple two‐step method for grafting thermoresponsive amine‐terminated poly(N‐isopropylacrylamide) brushes to thin films of...
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SubjectTerms 81.05.Rm
81.07.Pr
82.35.Gh
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Title Grafting stimuli-responsive polymer brushes to freshly-etched porous silicon
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